Cargando…
Applications in high resolution mass spectrometry : food safety and pesticide residue analysis /
Applications of High Resolution Mass Spectrometry: Food Safety and Pesticide Residue Analysis is the first book to offer complete coverage of all aspects of high resolution mass spectrometry (HRMS) used for the analysis of pesticide residue in food. Aimed at researchers and graduate students in food...
| Clasificación: | Libro Electrónico |
|---|---|
| Otros Autores: | , |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Amsterdam :
Elsevier,
[2017]
|
| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Front Cover; Applications in High Resolution Mass Spectrometry; Applications in HighResolution Mass Spectrometry: Food Safety and Pesticide Residue Analysis; Copyright; Contents; List of Contributors; Preface; 1
- HRMS: Fundamentals and Basic Concepts; 1.1 INTRODUCTION (TO HIGH-RESOLUTION MASS SPECTROMETRY); 1.1.1 BASIC CONCEPTS (UNITS AND DEFINITIONS); 1.1.2 LOW-RESOLUTION MASS SPECTROMETRY VERSUS HIGH-RESOLUTION MASS SPECTROMETRY; 1.2 RESOLUTION AND MASS RESOLVING POWER; 1.3 ACCURATE MASS MEASUREMENT: EXACT MASS AND MASS DEFECT; 1.4 MASS CALIBRATION IN HIGH-RESOLUTION MASS SPECTROMETRY.
- 1.5 GENERAL CONSIDERATIONSAcknowledgments; REFERENCES; 2
- HRMS: Hardware and Software; 2.1 INTRODUCTION; 2.2 PRINCIPLES OF HIGH-RESOLUTION MASS SPECTROMETRY ANALYZERS; 2.2.1 TIME-OF-FLIGHT; 2.2.2 FOURIER TRANSFORM ION CYCLOTRON RESONANCE; 2.2.3 ORBITRAP; 2.3 TIME-OF-FLIGHT MASS SPECTROMETRY: INSTRUMENT CONFIGURATION AND MAIN FEATURES; 2.3.1 STAND-ALONE ELECTROSPRAY IONIZATION TIME-OF-FLIGHT AND HYBRID QUADRUPOLE TIME-OF-FLIGHT INSTRUMENTATION; 2.3.2 IMPROVEMENTS OF CURRENT (QUADRUPOLE) TIME-OF-FLIGHT INSTRUMENTATION; 2.3.3 ION MOBILITY QUADRUPOLE TIME-OF-FLIGHT.
- 2.3.4 HYBRID ION TRAP TIME-OF-FLIGHT2.3.5 GAS CHROMATOGRAPHY-TIME-OF-FLIGHT AND GAS CHROMATOGRAPHY-QUADRUPOLE TIME-OF-FLIGHT; 2.4 ORBITRAP ANALYZERS: INSTRUMENT CONFIGURATIONS AND MAIN FEATURES; 2.5 ACQUISITION MODES IN HIGH-RESOLUTION MASS SPECTROMETRY; 2.5.1 DATA-DEPENDENT ACQUISITION; 2.5.2 DATA-INDEPENDENT ACQUISITION; 2.5.3 POSTACQUISITION APPROACHES; 2.6 DATABASES AND THE INTERNET RESOURCES FOR HIGH-RESOLUTION MASS SPECTROMETRY; Acknowledgments; REFERENCES; 3
- Analytical Strategies Used in HRMS; 3.1 INTRODUCTION; 3.2 ADVANTAGES OF HIGH-RESOLUTION MASS SPECTROMETRY IN PESTICIDE ANALYSIS.
- 3.2.1 SELECTIVITY IN HIGH-RESOLUTION MASS SPECTROMETRY: ACCURATE MASS AND RESOLUTION IN QUALITATIVE ANALYSIS3.2.2 IMPROVING SELECTIVITY BY TANDEM MASS SPECTROMETRY INFORMATION; 3.2.3 QUANTITATIVE PERFORMANCE; 3.3 DATA ANALYSIS WORKFLOWS IN HIGH-RESOLUTION MASS SPECTROMETRY; 3.3.1 QUALITATIVE SCREENING METHOD VALIDATION; 3.3.2 NONTARGET ANALYSIS; 3.4 CONCLUSIONS; Acknowledgments; REFERENCES; FURTHER READING; 4
- Current Legislation on Pesticides; 4.1 INTRODUCTION; 4.2 PESTICIDES; 4.2.1 IDENTITY AND PHYSICOCHEMICAL PROPERTIES; 4.2.2 PESTICIDES CLASSIFICATION.
- 4.2.3 PESTICIDE METABOLITES AND TRANSFORMATION PRODUCTS4.3 LEGISLATION; 4.3.1 PESTICIDES AUTHORIZATION; 4.3.2 MAXIMUM RESIDUE LIMITS; 4.3.3 MONITORING PROGRAMS; 4.4 ANALYTICAL QUALITY CONTROL-METHOD VALIDATION; 4.4.1 GUIDELINES FOR PESTICIDE RESIDUE ANALYSIS; 4.4.1.1 Method Validation for Pesticide Residues; 4.4.1.2 Quality Assurance; 4.4.1.3 Uncertainty; 4.5 MASS SPECTROMETRY IN PESTICIDE RESIDUE ANALYSIS; 4.5.1 MASS SPECTROMETRY IDENTIFICATION AND CONFIRMATION; 4.5.2 POTENTIAL OF HIGH-RESOLUTION MASS SPECTROMETRY IN PESTICIDE RESIDUE ANALYSIS; REFERENCES.
- 5
- Advanced Sample Preparation Techniques for Pesticide Residues Determination by HRMS Analysis.