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Reactions and mechanisms in thermal analysis of advanced materials /
Strong bonds form stronger materials. For this reason, the investigation on thermal degradation of materials is a significantly important area in research and development activities. The analysis of thermal stability can be used to assess the behavior of materials in the aggressive environmental con...
| Clasificación: | Libro Electrónico |
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| Otros Autores: | , |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Hoboken, New Jersey : Salem, Massachusetts :
John Wiley & Sons ; Scrivener Publishing,
2015.
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| Colección: | Materials Degradation and Failure Series
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| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Cover; Title Page; Copyright Page; Contents; Preface; Part 1: Degradation of Polymers; 1 Thermal Stability of Organic Monolayers Covalently Grafted on Silicon Surfaces; 1.1 Introduction; 1.1.1 Hydrogen-Terminated Si Surfaces; 1.2 Alkyl-Grafted Surfaces; 1.2.1 Preparation; 1.2.2 Thermal Stability of Alkyl-Grafted Surfaces; 1.2.3 Case of Substituted Alkyl Surfaces; 1.3 Alkoxy-Grafted Surfaces; 1.3.1 Preparation; 1.3.2 Thermal Stability of Alkoxy-Grafted Surfaces; 1.4 Surfaces Grafted with Aryl Groups; 1.4.1 Preparation; 1.4.2 Thermal Stability; 1.5 Surfaces Grafted via Si-N Linkages.
- 1.5.1 Preparation1.5.2 Thermal Stability; 1.5.2.1 The Thermal Treatment of the Si Surface with NH3; 1.5.2.2 Thermal Stability of the Modified Surfaces; 1.6 Summary; References; 2 Thermal Analysis to Discriminate the Stability of Biomedical Ultrahigh-Molecular-Weight Polyethylenes Formulations; 2.1 Introduction; 2.2 Suitability of TGA Analysis for the Study of Stability of Medical Polyethylene; 2.2.1 Introduction; 2.2.2 Degradation Curves of UHMWPE Depending on the Reaction Atmosphere; 2.2.3 Decomposition Processes of UHMWPE in Air; 2.2.3.1 Thermo-oxidation Process.
- 2.2.3.2 Thermal Degradation Process of UHMWPE2.2.4 Irradiation Effects on the Thermogravimetric Curves of UHMWPE; 2.2.5 Stabilization of Polyethylene against Thermo-oxidative Degradation; 2.3 Activation Energies of Degradation Processes in the Thermal Decomposition of UHMWPE; References; 3 Materials Obtained by Solid-State Thermal Decomposition of Coordination Compounds and Metal-Organic Coordination Polymers; 3.1 Introduction; 3.2 Coordination Compounds and Metal-Organic Coordination Polymers as Precursors of Oxides; 3.2.1 Coordination Compounds with Carboxylic Acid as Ligand.
- 3.2.2 Coordination's Compounds as Precursors in the Combustion Synthesis of Oxides3.2.3 Metal-Organic Coordination Polymers as Precursors of Oxides; 3.3 Coordination Compounds and Metal-Organic Coordination Polymers as Precursors of Sulfides; 3.4 Coordination Compounds as Precursors of Composites; 3.5 Coordination Compounds and Metal-Organic Coordination Polymers as Precursors of New Complexes; 3.6 Coordination Compounds and Metal-Organic Coordination Polymers as Precursor of Metals; 3.7 Coordination Compounds as Precursor of Nitrides; 3.8 Other Materials; 3.9 Conclusions; References.
- 4 Methods for Limiting the Flammability of High-Density Polyethylene with Magnesium Hydroxide4.1 Introduction; 4.2 Experimental Part; 4.2.1 Materials; 4.2.2 Sample Preparation; 4.2.3 Methods of Testing; 4.3 Results and Discussion; 4.3.1 Thermal Stability; 4.3.2 Flammability; 4.3.2.1 UL-94 Test; 4.3.2.2 Limiting Oxygen Index (LOI); 4.3.2.3 Cone Calorimetry; 4.3.3 Mechanical Properties; 4.3.4 Microstructure of Fracture Surface of Composites; 4.4 Conclusions; References; 5 Thermal Analysis in the Study of Polymer (Bio)-degradation; 5.1 Introduction; 5.2 Differential Scanning Calorimetry.