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Multidimensional analytical techniques in environmental research /
| Clasificación: | Libro Electrónico |
|---|---|
| Otros Autores: | , |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Amsterdam :
Elsevier,
2020.
|
| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Intro
- Multidimensional Analytical Techniques in Environmental Research
- Copyright
- Contents
- Contributors
- Chapter 1: Multidimensional analytical techniques in environmental research: Evolution of concepts
- Challenges in environmental research
- Coping with environmental organic matrices complexity
- Multidimensional nuclear magnetic resonance (NMR) spectroscopy in environmental research
- Solution-state NMR spectroscopy in environmental research
- Solid-state NMR spectroscopy in environmental research
- Comprehensive multiphase and in vivo NMR for analysis of natural samples
- High-resolution mass spectrometry in environmental research
- Two-dimensional correlation spectroscopy in environmental research
- Fluorescence spectroscopy in the characterization of environmental samples
- Comprehensive two-dimensional chromatography in environmental analysis
- Synchrotron-based techniques as multidimensional analytical tools
- Conclusions
- Acknowledgments
- References
- Chapter 2: Environmental solution-state NMR spectroscopy: Recent advances, potential, and impacts
- Introduction
- NMR methodology
- Operating principle
- NMR spectrometer
- NMR methods
- 1D 1H and 13C NMR
- 2D 1H1H and 1H13C NMR
- 3D 1H1H13C NMR
- Soil organic matter analysis
- Characteristics of soil organic matter and humic substances
- SOM samples preparation
- NMR characterization
- Solution-state NMR spectroscopy of dissolved organic matter in water bodies and sediments
- Characteristics of dissolved organic matter
- DOM sample preparation
- NMR characterization
- Solution-state NMR spectroscopy of organic matter in air and rainwater
- Characteristic of atmospheric organic matter (organic aerosols)
- NMR sample preparation
- NMR characterization
- Processing of environmental NMR data
- NMR spectral analysis software
- Functional analysis
- Factorial analysis
- Challenges in environmental NMR metabolomics
- Recent advances in environmental NMR
- References
- Chapter 3: Advanced two-dimensional solid-state NMR spectroscopy and its application in environmental sciences
- Introduction to nuclear magnetic resonance
- Overview
- NMR theory
- Solid-state NMR
- 2D solid-state NMR spectroscopy
- Basics of 2D NMR
- Advanced 2D solid-state NMR techniques
- 2D 1H-13C heteronuclear correlation (HETCOR) solid-state NMR
- HETCOR for identification of functional groups
- HETCOR for connectivity
- HETCOR for domains and heterogeneities
- 2D solid-state 13C-13C correlation NMR
- Summary and outlook
- References
- Chapter 4: High-resolution mass spectrometry strategies for the investigation of dissolved organic matter
- Motivation
- Environmental production and processing of DOM with regards to individual analytes
- HRMS strategies for the investigation of DOM
- Sample preparation