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Nanodiamonds : advanced material analysis, properties and applications /
| Clasificación: | Libro Electrónico |
|---|---|
| Otros Autores: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Saint Louis :
Elsevier,
2017.
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| Colección: | Micro & nano technologies.
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| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Front Cover; Nanodiamonds; Copyright; Contents; Contributors; About the Editor; Preface; About the Authors; 1 General properties of diamond; 1.1 Introduction; 1.2 Properties of insulating diamond; Hole mobility, drift velocity, and effective mass; Electron mobility, drift velocity, and effective mass; 1.3 Properties of doped diamond; Electronic properties of p-type diamond; Hole and electron effective density of state masses; Hole effective masses; Free hole density for p> ND; Hole conductivity; Electronic properties of n-type diamond.
- The free electron densityElectron effective mass; Electron Hall mobilities; n-type conductivity; 1.4 Summary; References; 2 Production and purification of nanodiamonds; 2.1 Introduction; 2.2 Types of nanodiamonds and methods of nanodiamond synthesis; 2.2.1 Nanodiamond particles produced by detonation shock-wave-assisted synthesis; 2.2.1.1 Nanodiamond produced from high energy explosives; 2.2.1.2 Nanodiamond produced from carbon and carbon/explosive mixture; 2.2.2 HPHT nanodiamonds; 2.2.3 Laser-assisted synthesis of nanodiamond; 2.2.4 Other methods of synthesis of nanodiamond.
- 2.3 Nanodiamond purification from sp2 carbon and metal impurities2.4 Disaggregation, crushing, and fractionation of nanodiamond; 2.4.1 Disaggregation techniques; 2.4.1.1 Ball milling; 2.4.1.2 Jet milling; 2.4.1.3 Thermal and chemical treatments; 2.4.1.4 Ultrasonic disaggregation and dispersion; 2.4.1.5 Specialty techniques & recent advancements; Bead assisted sonic disintegration (BASD); Matrix assisted milling/crushing; 2.4.2 Fractionation; 2.5 Doping of nanodiamond particles; 2.6 Conclusion and future outlook; References; Acknowledgement.
- 3 Structure, shape, defects and impurities in nanodiamonds investigated by HRTEM and STEM-EELS3.1 Imaging structure, morphology, and defects in nanodiamonds by TEM; 3.1.1 Introduction; 3.1.2 Bright-field TEM Imaging and electron diffraction of nanodiamond material; 3.1.3 High resolution TEM imaging; 3.1.4 Scanning transmission electron microscopy; 3.2 Probing the electronic structure of diamond and its dopants by Electron Energy-Loss Spectroscopy; 3.2.1 Introduction; 3.2.2 Low-loss EELS; 3.2.3 Core-loss EELS; 3.2.3.1 Nanodiamond carbon K-edge ELNES; 3.2.3.2 Monochromatic EELS data.
- 3.2.3.3 Nitrogen detection by core-loss EELS3.2.3.4 Boron detection by core-loss EELS; 3.3 Imaging and spectroscopy of nanodiamond surface functionalization; References; 4 Raman investigations on nanodiamonds; 4.1 Introduction and scope; 4.2 Methodology and experimental issues; 4.3 Characteristic features of the Raman spectra of NDs
- similarities and differences; 4.4 The diamond line profile
- phonon confinement; 4.5 Low frequency broad signals
- core shell model; 4.6 Raman spectroscopy of detonation nanodiamonds; 4.6.1 Wavelength dependent effects: UV excitations.