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Electrochemistry of dihydroxybenzene compounds : carbon based electrodes and their uses in synthesis and sensors /
| Clasificación: | Libro Electrónico |
|---|---|
| Autores principales: | , , |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Amsterdam, Netherlands :
Elsevier,
[2017]
|
| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Front Cover; Electrochemistry of Dihydroxybenzene Compounds; Copyright Page; Contents; List of Figures; List of Tables; List of Schemes; Acknowledgments; List of Abbreviations and Symbols; 1 Introduction; 1.1 Nanotechnology and Nanoscience; 1.1.1 Type and Properties of Nanostructures; 1.1.2 Applications of Nanomaterials; 1.2 Carbon-Based Materials; 1.2.1 Carbon-Based Materials in Electrochemistry; 1.3 The Importance of Electrode Surface in Electrochemistry; 1.3.1 Multiwalled Carbon Nanotube; 1.3.2 Graphene.
- 1.3.3 Benefits of Applying Carbon Nanotubes (CNTs) and Graphene in Electrochemical Analysis1.4 Polymer Nanocomposite (PNC) Based on Carbon Nanomaterial Electrode; 1.4.1 PNC Based on Multiwalled Carbon Nanotube (MWCNT); 1.4.2 PNC Based on Graphene; 1.5 Conductive Polymer; 1.5.1 Types of Conducting Polymers; 1.5.2 Poly(4-vinylpyridine) (P4VP) as a Conducting Polymer; 1.6 Electroorganic Synthesis; 1.7 Dihydroxybenzenes and Its Derivatives; 1.7.1 Catechol; 1.7.2 Hydroquinone; 1.8 Electrochemical Synthesis of CT in the Presence of Nucleophile; 1.8.1 Thiosemicarbazide.
- 1.9 Methods Used for Determination of Dihydroxybenzene (DHB)1.9.1 Electrochemical Method; 1.10 Electrochemical Sensors for Analysis; 1.10.1 CT as a Sensor for Electrochemical Determination; 1.10.2 Electrochemical Sensor for Detection of CT and HQ; 1.10.2.1 Determination of Catechol; 1.10.2.2 Determination of Hydroquinone; 1.10.2.3 Simultaneous Determination of CT and HQ on Modified Electrodes; 1.11 Application of the Nanocomposite-Modified Electrodes for Pharmaceutical Analysis; 1.11.1 Determination of Paracetamol (PCT); 1.11.2 Determination of Acetylsalicylic Acid (ASA).
- 1.11.3 Determination of Caffeine1.12 Problem Statement; 1.13 Objectives; 2 Experimental; 2.1 Materials; 2.2 Instruments; 2.3 Electrochemical Method for Synthesis of Dihydroxybenzenes Derivatives; 2.3.1 Preparation of Working Electrode; 2.3.2 Electrochemical Study of CT in the Presence of TSC; 2.3.3 Electroorganic Synthesis; 2.4 Electrochemical Study of Modified Electrodes; 2.4.1 Purification and Acetic Functionalization of MWCNTs; 2.4.2 Preparation of P4VP/MWCNT-Modified GCE; 2.4.3 Graphene Sheets Functionalization; 2.4.4 Preparation of P4VP/GR-Modified GCE.
- 2.5 Determination of TSC in Real Samples2.5.1 Determination of TSC in Water Samples; 2.5.2 Determination of TSC in Propranolol Tablets; 2.6 Electrochemical Sensor Studies; 2.6.1 Electrochemistry Determination of Diphenols; 2.6.2 Electrochemistry of PCT; 2.6.3 Electrochemistry of Aspirin and Caffeine; 2.7 Real Sample Analysis; 2.7.1 Determination of Diphenols in Water Samples; 2.7.2 Determination of PCT in Formulation Tablets; 2.7.3 Determination of PCT in Urine Mid-Samples; 2.7.4 Determination of ASA in Formulation Tablets; 2.8 Characterization of the Modified Electrodes.