Microwave-assisted sample preparation for trace element determination /

Microwave-Assisted Sample Preparation for Trace Element Analysis describes the principles, equipment, and applications involved in sample preparation with microwaves for trace element analysis. The book covers well-established applications as well as new trends in this field. Hot topics such as samp...

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Detalles Bibliográficos
Clasificación:Libro Electrónico
Otros Autores: Flores, �Erico Marlon Moraes (Editor )
Formato: Electrónico eBook
Idioma:Inglés
Publicado: Amsterdam : Elsevier, 2014.
Temas:
Trace elements > Analysis.
Sample preparation (Chemistry)
Microwaves > Scientific applications.
Analytic Sample Preparation Methods
Pr�eparation de l'�echantillon (Chimie)
Micro-ondes > Applications scientifiques.
SCIENCE > Life Sciences > Biology.
Trace elements > Analysis
Acceso en línea:Texto completo
Tabla de Contenidos:
  • Front Cover; Microwave-Assisted Sample Preparation for Trace Element Determination; Copyright; Contents; Preface; List of Contributors; Chapter 1
  • Introduction to Sample Preparation for Trace Element Determination; 1.1. INTRODUCTION; 1.2. THE ANALYTICAL SEQUENCE; 1.3. ANALYTICAL EFFICIENCY AND ROBUSTNESS; 1.4. SYSTEMATIC ERRORS IN SAMPLE PREPARATION; 1.5. PRELIMINARY PROCESSES, TREATMENTS; 1.6. COMMENTS ON CONVENTIONAL OPEN AND CLOSED SYSTEMS FOR SAMPLE PREPARATION; 1.7. CONCLUSION; REFERENCES; Chapter 2
  • Microwave Heating; 2.1. INTRODUCTION.
  • 2.2. GENERAL ASPECTS OF ENERGY AND MATTER INTERACTION2.3. DIELECTRIC HEATING; 2.4. ADDITIONAL ASPECTS TO CONSIDER IN MICROWAVE HEATING; 2.5. MICROWAVE HEATING IN SAMPLE PREPARATION; 2.6. FINAL REMARKS; REFERENCES; Chapter 3
  • Systems for Microwave-Assisted Wet Digestion; 3.1. INTRODUCTION; 3.2. OPEN SYSTEMS; 3.3. CLOSED SYSTEMS; 3.4. HISTORY OF MICROWAVE SYSTEMS AND CURRENT TECHNOLOGY; 3.5. FLOW SYSTEMS; 3.6. FINAL REMARKS AND FUTURE TRENDS; REFERENCES; Chapter 4
  • Wet Digestion Using Microwave Heating; 4.1. MICROWAVE-ASSISTED WET SAMPLE DIGESTION.
  • 4.2. DEVELOPMENT AND EVALUATION OF MICROWAVE-ASSISTED WET DIGESTION PROCEDURES4.3. APPLICATIONS OF MICROWAVE-ASSISTED PROCEDURES FOR SAMPLE DIGESTION; REFERENCES; Chapter 5
  • Microwave-Induced Combustion; 5.1. INTRODUCTION; 5.2. COMBUSTION SYSTEMS FOR SAMPLE DIGESTION; 5.3. APPARATUS AND PROCEDURES FOR MIC; 5.4. FOCUSED MICROWAVE-INDUCED COMBUSTION; 5.5. ABSORBING SOLUTIONS; 5.6. ALTERNATIVE USES OF MIC; 5.7. FINAL REMARKS; REFERENCES; Chapter 6
  • Diluted Acids in Microwave-Assisted Wet Digestion; 6.1. INTRODUCTION; 6.2. DILUTED ACIDS IN MICROWAVE-ASSISTED WET DIGESTION IN CLOSED VESSELS.
  • 6.3. OTHER STRATEGIES TO REDUCE THE AMOUNTS OF ACIDS FOR DIGESTION6.4. FINAL REMARKS; REFERENCES; Chapter 7
  • Microwave-Assisted Ultraviolet Digestion; 7.1. INTRODUCTION; 7.2. MW-UV METHOD; 7.3. COMMERCIAL SYSTEMS FOR MW-UV; 7.4. APPLICATIONS IN CHEMISTRY; 7.5. FINAL CONSIDERATIONS; REFERENCES; Chapter 8
  • Microwave-Assisted Extraction; 8.1. INTRODUCTION; 8.2. PRINCIPLES AND TECHNOLOGIES; 8.3. CURRENT APPLICATIONS; REFERENCES; Chapter 9
  • Flow Digestion Systems with Microwave and Conductive Heating; 9.1. SYSTEMATIC ERRORS IN SAMPLE DIGESTION: GENERAL ASPECTS RELATED TO FLOW DIGESTION.
  • 9.2. DELETERIOUS EFFECTS OF CARBON IN ICP-BASED ELEMENTAL ANALYSIS9.3. PRINCIPLES OF FLOW DIGESTION SYSTEMS; 9.4. FLOW DIGESTION AT AMBIENT PRESSURE; 9.5. FLOW DIGESTION AT MEDIUM PRESSURE; 9.6. HIGH-PRESSURE FLOW DIGESTION SYSTEMS; 9.7. COMPONENTS OF FLOW DIGESTION SYSTEMS; 9.8. STRUCTURAL MATERIALS AND DISSOLUTION REAGENTS FOR FLOW DIGESTION SYSTEMS; 9.9. FLOW DIGESTION OF SLURRIES; REFERENCES; Chapter 10
  • Microwave-Assisted Sample Preparation for Element Speciation; 10.1. INTRODUCTION; 10.2. MERCURY SPECIATION; 10.3. ORGANOTIN SPECIATION; 10.4. SELENIUM SPECIATION.

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