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Separation methods in organic chemistry and biochemistry /
Separation Methods in Organic Chemistry and Biochemistry aims to provide perspectives for the commonly used separations methods and to discuss indications for their use. The book discusses the determination of molecular properties useful in separation based on micro test methods, paper chromatograph...
| Clasificación: | Libro Electrónico |
|---|---|
| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
New York :
Academic Press,
1969.
|
| Temas: | |
| Acceso en línea: | Texto completo |
MARC
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| 020 | |a 1483220680 |q (electronic bk.) | ||
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| 020 | |z 9780127616506 | ||
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| 100 | 1 | |a Wolf, Frank James, |d 1916- | |
| 245 | 1 | 0 | |a Separation methods in organic chemistry and biochemistry / |c Frank J. Wolf. |
| 264 | 1 | |a New York : |b Academic Press, |c 1969. | |
| 300 | |a 1 online resource (viii, 237 pages) : |b illustrations | ||
| 336 | |a text |b txt |2 rdacontent | ||
| 337 | |a computer |b c |2 rdamedia | ||
| 338 | |a online resource |b cr |2 rdacarrier | ||
| 504 | |a Includes bibliographical references. | ||
| 588 | 0 | |a Print version record. | |
| 506 | |3 Use copy |f Restrictions unspecified |2 star |5 MiAaHDL | ||
| 533 | |a Electronic reproduction. |b [Place of publication not identified] : |c HathiTrust Digital Library, |d 2011. |5 MiAaHDL | ||
| 538 | |a Master and use copy. Digital master created according to Benchmark for Faithful Digital Reproductions of Monographs and Serials, Version 1. Digital Library Federation, December 2002. |u http://purl.oclc.org/DLF/benchrepro0212 |5 MiAaHDL | ||
| 583 | 1 | |a digitized |c 2011 |h HathiTrust Digital Library |l committed to preserve |2 pda |5 MiAaHDL | |
| 505 | 0 | |6 880-01 |a Front Cover; Separation Methods in Organic Chemistry and Biochemistry; Copyright Page; Preface; Table of Contents; Introduction; I. TYPES OF SEPARATION CONSIDERED; II. DISTRIBUTION COEFFICIENT; A. Group Separation; B. Fractionation Separations-Reasons for Using Them; C. Methods of Fractionation; III. USE OF MICRO METHODS; IV. EVALUATION OF SEPARATION PROCESSES; Chapter I. General Principles; I. STABILITY; II. GROUP SEPARATIONS; A. Molecular Size; 1. Dialysis and Ultrafiltration; 2. Gel Filtration; B. Ionic Properties; 1. Ion Exchange; 2. Solvent Extraction; C. Polarity. | |
| 505 | 8 | |a 1. Definition and General Principles2. Solvent Extraction; D. Summation of Group Properties and Methods; III. FRACTIONATION SEPARATIONS; A. Requirements and General Methods; B. Countercurrent Distribution; 1. Procedure; 2. Parameters of the Separation Process-Relationship of Chromatography and Countercurrent Distribution; 3. Mathematical Description-Formation and Location of Bands; 4. Mathematical Description-Band Spread and Separation; chapter II. Determination of Molecular Properties; I. INTRODUCTION; II. CHROMATOGRAPHIC PROCEDURES; A. Visualization; 1. Direct Visualization. | |
| 505 | 8 | |a Chapter Ill. Solvent ExtractionI. PARTITION RATIO; A. Definition; B. Chemical Potential; 1. Activity Coefficient; 2. Relationship between Different Solvent Systems; I. Partition Ratio; C. Methods of Determining the Partition Ratio; 1. Paper Chromatography; 2. Equilibration between Two Phases; 3. Other Procedures; II. APPLICATION OF SOLVENT EXTRACTION FOR GROUP SEPARATION; A. Solvent Properties; 1. Partition Ratio; 2. Solvent Polarity; 3. Solvent Removal and Loss; 4. Reactivity; 5. Ease of Separation; B. Solvent Removal Methods; 1. Evaporation; 2. Back Extraction; 3. Adsorption. | |
| 505 | 8 | |a 4. PrecipitationIII. APPLICATION OF SOLVENT EXTRACTION FOR FRACTIONATION SEPARATION; IV. PARTITION CHROMATOGRAPHY; A. Properties of the Solid Support; B. Properties of the Solvent System; 1. Stability; 2. Partition Ratio; 3. Factors Influencing Column Load; C. Mechanical Problems; D. Mechanism of Separation; 1. Factors Influencing Plate Height in Columns; E. Applications of Partition Chromatography; 1. Insulin; 2. Aldosterone; 3. Use of Hydrophilic Gels; 4. Miscellaneous Applications; V. COUNTERCURRENT DISTRIBUTION; A. Physical and Chemical Requirements; 1 . Solvent System. | |
| 520 | |a Separation Methods in Organic Chemistry and Biochemistry aims to provide perspectives for the commonly used separations methods and to discuss indications for their use. The book discusses the determination of molecular properties useful in separation based on micro test methods, paper chromatography, thin-layer chromatography, and electrophoresis. The text then describes the theoretical principles of group-separation procedures, liquid-liquid partition, ion-exchange selectivity, gel permeation, and adsorption. Methods of influencing the selectivity coefficients, the basic theory of fractionat. | ||
| 650 | 0 | |a Separation (Technology) | |
| 650 | 0 | |a Chemistry, Organic. | |
| 650 | 0 | |a Biochemistry. | |
| 650 | 2 | |a Biochemistry |0 (DNLM)D001671 | |
| 650 | 2 | |a Chemistry Techniques, Analytical |0 (DNLM)D002623 | |
| 650 | 2 | |a Chemistry, Organic |0 (DNLM)D002625 | |
| 650 | 6 | |a S�eparation (Technologie) |0 (CaQQLa)201-0000375 | |
| 650 | 6 | |a Chimie organique. |0 (CaQQLa)201-0004956 | |
| 650 | 6 | |a Biochimie. |0 (CaQQLa)201-0001077 | |
| 650 | 7 | |a organic chemistry. |2 aat |0 (CStmoGRI)aat300054541 | |
| 650 | 7 | |a biochemistry. |2 aat |0 (CStmoGRI)aat300054538 | |
| 650 | 7 | |a SCIENCE |x Chemistry |x Organic. |2 bisacsh | |
| 650 | 7 | |a Biochemistry |2 fast |0 (OCoLC)fst00831961 | |
| 650 | 7 | |a Chemistry, Organic |2 fast |0 (OCoLC)fst00853501 | |
| 650 | 7 | |a Separation (Technology) |2 fast |0 (OCoLC)fst01112723 | |
| 650 | 7 | |a Trennverfahren |2 gnd |0 (DE-588)4078395-9 | |
| 650 | 7 | |a Methode |2 gnd |0 (DE-588)4038971-6 | |
| 650 | 7 | |a Organische Chemie |2 gnd |0 (DE-588)4043793-0 | |
| 650 | 7 | |a Biochemie |2 gnd |0 (DE-588)4006777-4 | |
| 650 | 1 | 7 | |a Scheidingstechnieken. |2 gtt |
| 650 | 1 | 7 | |a Chromatografie. |2 gtt |
| 650 | 1 | 7 | |a Biomoleculen. |2 gtt |
| 650 | 7 | |a S�eparation (technologie) |2 ram | |
| 650 | 7 | |a Biochimie. |2 ram | |
| 776 | 0 | 8 | |i Print version: |a Wolf, Frank James, 1916- |t Separation methods in organic chemistry and biochemistry |z 0127616500 |w (DLC) 71084256 |w (OCoLC)26211 |
| 856 | 4 | 0 | |u https://sciencedirect.uam.elogim.com/science/book/9780127616506 |z Texto completo |
| 880 | 8 | |6 505-01/(S |a 2. Chemical Tests3. Bioautography; 4. Reactivity or Effect on a Test System; III. MICRO TESTS; A. Type and Sequence of Tests; 1. Solvent Extraction; 2. Ion Exchange; B. Compound Groups; C. Determination of Approximate Dissociation Constant and pK; 1. Introduction; 2. Solvent Extraction; 3. Paper and Thin-Layer Chromatography; 4. Ion Exchange; 5. Electrophoresis; D. Polarity; 1. Introduction; 2. Polarity Scale; E. Molecular Size; 1. Introduction; 2. Dialysis; 3. Gel Permeation; F. Functional Group Determinations; 1. Introduction and Theory; 2. Rm and ΔRm; 5. Acidic and Basic Groups; G. Summary. | |