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Experimental inorganic/physical chemistry : an investigative, integrated approach to practical project work /
"This comprehensive book combines all instrumental and radiochemical techniques with qualitative and quantitative (volumetric and gravimetric) analyses, and also with preparation of compounds. This strengthens both analytical and preparative skills. All main elements and groups of the periodic...
| Clasificación: | Libro Electrónico |
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| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Chichester :
Horwood Pub.,
1999.
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| Colección: | Horwood series in chemical science.
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| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Front Cover; Mounir A. Malati; Experimental Inorganic/Physical Chemistry: An Investigative, Integrated Approach to Practical Project Work; Copyright Page; Dedication; Preface; List of Abbreviations; Table of Contents; Chapter 1. Good Safe Laboratory Practice; 1.1 INTRODUCTION; 1.2 USE AND CARE OF GLASSWARE; 1.3 USE OF OTHER LABWARE; 1.4 WEIGHING; 1.5 HEATING; 1.6 INTRODUCTION TO SAFETY; 1.7 WARNING SYMBOLS; 1.8 RISK AND SAFETY PHRASES; 1.9 EXPLOSIONS AND FIRES; 1.10 FIRE EXTINGUISHERS; 1.11 SPILLAGE TREATMENT; 1.12 WASTE DISPOSABLE; 1.13 CAREFUL USE OF CONCENTRATED ACIDS AND ALKALIS.
- 1.14 HANDLING ORGANIC SOLVENTS1.15 SOME SIMPLE TESTS AND OPERATIONS; References; Chapter 2. Techniques; 2.1 CHARACTERISATION OF SOLIDS; 2.2 TITRIMETRY USING INDICATORS; 2.3 GRAVIMETRY; 2.4 SPECTROSCOPIC METHODS; 2.5 ELECTROCHEMICAL METHODS; 2.6 THERMAL METHODS; 2.7 SOLVENT EXTRACTION AND ION EXCHANGE; 2.8 CHROMATOGRAPHY; 2.9 CONTROLLED ATMOSPHERE TECHNIQUES; 2.10 PHOTOCHEMICAL METHODS; 2.11 STUDY OF KINETICS OF REACTIONS; 2.12 NUCLEAR AND RADIOCHEMICAL TECHNIQUES; References; Chapter 3. The s Block Metals; 3.1 INTRODUCTION; 3.2 QUALITATIVE TESTS; 3.3 ANALYTICAL CHEMISTRY OF THE ALKALI METALS.
- 3.4 ANALYTICAL CHEMISTRY OF GROUP 2 METALS3.5 SURFACE CHEMICAL STUDY OF THE s BLOCK; Chapter 4. Boron and Aluminium; 4.1 INTRODUCTION; 4.2 QUALITATIVE TESTS; 4.3 ANALYTICAL CHEMISTRY OF BORON; 4.4 PREPARATION AND CHARACTERISATION OF BORON COMPLEXES; 4.5 ANALYTICAL CHEMISTRY OF ALUMINIUM; 4.6 COMPLEX COMPOUNDS OF ALUMINIUM; Chapter 5. The Carbon Group; 5.1 INTRODUCTION; 5.2 QUALITATIVE TESTS ON C, Si AND THEIR COMPOUNDS; 5.3 ANALYTICAL CHEMISTRY OF CARBON COMPOUNDS; 5.4 PHOTOCATALYSED REDUCTION OF CARBONATE; 5.5 ANALYTICAL CHEMISTRY OF SILICATES.
- 5.6 SURFACE CHEMICAL STUDY OF PRECIPITATED SILICA5.7 QUALITATIVE TESTS ON TIN AND ITS COMPOUNDS; 5.8 ANALYTICAL CHEMISTRY OF TIN; 5.9 PREPARATION AND ANALYSIS OF TIN IODIDES; 5.10 COMPLEX COMPOUNDS OF TIN; 5.11 QUALITATIVE TESTS ON LEAD AND ITS COMPOUNDS; 5.12 ANALYTICAL CHEMISTRY OF LEAD; 5.13 COMPLEX COMPOUNDS OF LEAD; 5.14 THE PHOTOCATALYSED REMOVAL OF LEAD IONS FROM SOLUTION; Chapter 6. The Nitrogen Group; 6.1 INTRODUCTION; 6.2 QUALITATIVE TESTS ON NITROGEN COMPOUNDS; 6.3 ANALYTICAL CHEMISTRY OF NITROGEN COMPOUNDS; 6.4 THE U.V.-ENHANCED DECOMPOSITION OF AMMONIUM NITRITE.
- 6.5 PREPARATION AND REACTIONS OF DINITROGEN TETROXIDE6.6 INVESTIGATING THE REACTIONS OF HYDRAZINIUM AND HYDROXYLAMMONIUM SALTS; 6.7 AMMONIA AND NITRITE AS LIGANDS; 6.8 LIQUID AMMONIA; 6.9 QUALITATIVE TESTS ON PHOSPHORUS AND ITS COMPOUNDS; 6.10 ANALYTICAL CHEMISTRY OF PHOSPHATES AND ORTHOPHOSPHORIC ACID; 6.11 POTENTIOMETRIC TITRATION OF PHOSPHONIC ACID; 6.12 QUALITATIVE TESTS ON ANTIMONY AND BISMUTH; 6.13 ANALYTICAL CHEMISTRY OF ANTIMONY AND BISMUTH; 6.14 PREPARATION AND REACTIONS OF [PCI4][SbCI6]; 6.15 EFFECT OF Bi(III) ON THE OXIDATION OF Cr(III) EDTA COMPLEX BY PERMANGANATE.