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Pulse methods in 1D and 2D liquid-phase NMR /
FROM THE PREFACE: Pulse Methods in 1D and 2D Liquid-Phase NMR is written to enable the practicing NMR spectroscopist to understand and apply the varied and powerful new techniques developed in the past few years for obtaining spectra with greatly increased information content and from smaller and sm...
| Clasificación: | Libro Electrónico |
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| Otros Autores: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
San Diego, Calif. :
Academic Press,
�1988.
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| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Front Cover; Pulse Methods in 1D and 2D Liquid-Phase Nmr; Copyright Page; Table of Contents; Preface; CHAPTER 1. Basic Methods and Simple Pulsed Experiments; I. Introduction; II. Spin-Echo Experiments; III. Polarization-Transfer Experiments; IV. Experimental Aspects of Pulsed NMR; References; CHAPTER 2. Density-Operator Theory of Pulses and Precession; I. Introduction; II. Overview; III. Theory and Use of Product Operators; IV. A Typical Two-Dimensional Experiment-Double-Quantum Spectroscopy of Two Coupled Spins-1/2; V. Summary; Acknowledgments; References
- CHAPTER 3. Polarization Transfer and Editing Techniques*I. Introduction; II. Theory; III. Polarization Transfer and Purging; IV. Heteronuclear Spectral Editing Techniques; Appendixes; Acknowledgment; References; CHAPTER 4. Principles of Multiple-Quantum Spectroscopy; I. Introduction; II. Operator Formalism; III. Multiple-Quantum Coherence for a System of Two Spin-1/2 Nuclei; IV. Order-Selective Detection; V. Multiple-Quantum Coherences for Systems Containing Three or More Spin-1/2 Nuclei; VI. Summary; Acknowledgments; References
- CHAPTER 5. Applications of Two-Dimensional NMR Experiments in LiquidsI. Introduction; II. Instrumental Requirements; III. J-Resolved 2D NMR; IV. Chemical Shift Correlation 2D NMR; V. Shift Correlation by Relayed Coherence-Transfer 2D NMR; VI. Magnetization-Transfer 2D NMR; VII. Zero- and Multiple-Quantum 2D Methods; References; CHAPTER 6. Applications of 2D NMR to Biological Systems; I. Introduction; II. The Basic 2D NMR Experiments for Spectral Assignment and Structure Elucidation; III. Advanced Methods for Biological Samples; IV. Structural Analysis of Biomolecules; References
- CHAPTER 7. Multiple-Resonance and Two-Dimensional NMR Techniques in Analysis of Fluorocarbon Compounds and PolymersI. Introduction; II. Resolution Enhancement and Proton Decoupling; III. Two-Dimensional NMR; IV. Experimental Details; V. Summary; References; CHAPTER 8. Recent Developments in Pulsed NMR Methods; I. RELAY and Observation by Hydrogen Detection; II. Homonuclear Correlation; III. Isotropic Mixing Experiments; IV. Applications of Zero-Quantum Coherence; V. Nuclear Overhauser Enhancement; References; Appendix: Reading List; Index