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Organic functional group analysis theory and development,
Organic Functional Group Analysis: Theory and Development details the methods the best represent the progress in functional group analysis. In the second part, the title presents several papers that cover various areas in the field of functional group analysis. The text first covers the oximation of...
| Clasificación: | Libro Electrónico |
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| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Oxford, New York,
Pergamon Press
[1968]
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| Edición: | [1st ed.]. |
| Colección: | The Commonwealth and international library. Selected readings in analytical chemistry
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| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Front Cover; Organic Functional Group Analysis: Theory and Development; Copyright Page; Table of Contents; Preface; PART I:; CHAPTER 1. Determination of the Carbonyl Group: Oximation and Other Methods; EARLY OXIMATION METHODS; OXIMATION EQUILIBRIA AND pH; MODERN OXIMATION METHODS; RATE OF OXIMATION AND pH; FUTURERE SEARCH: NEW APPLICATIONS AND METHODS; OTHER CARBONYL METHODS; REFERENCES; CHAPTER 2. Analysis of Enolic-type Compounds: Kurt Meyer Bromination and Nonaqueous Titration; BROMINATION OF THE ENOL TAUTOMER; NONAQUEOUS TITRATION OF ENOLIC COMPOUNDS; REFERENCES
- CHAPTER 3. Determination of the Hydroxyl and Amino Groups: Base-catalyzed Acylation MethodsEARLY ACYLATION METHODS; BASE-CATALYZED HYDROLYSIS OF ACETIC ANHYDRIDE; MODERN ACYLATION METHODS; STERIC HINDRANCE PROBLEMS: TERTIARY ALCOHOLS AND ORTHO-SUBSTITUTED PHENOLS; FUTURE RESEARCH: APPLICATIONS TO INSTRUMENTAL ANALYSIS; REFERENCES; CHAPTER 4. Determination of Hydroxyl Groups and Alkoxysilanes: Acid-catalyzed Acetylation Methods; EARLY ACID-CATALYZED ACETYLATION METHODS; MECHANISM OF ACID-CATALYZED ACETYLATION; MODERN METHODS: DETERMINATION OF HYDROXYL GROUPS
- MODERN METHODS AND STERICALLY-HINDERED HYDROXYL GROUPSMODERN METHODS: DETERMINATION OF ALKOXYSILANES; APPLICATIONS TO INSTRUMENTAL ANALYSIS AND FUTURE RESEARCH; REFERENCES; CHAPTER 5. Determination of the Epoxide Group: Quantitative Ring Opening Methods; EARLY ACID ADDITION METHODS; MODERN ACID ADDITION METHODS; NUCLEOPHILIC REACTIONS IN NEUTRAL OR BASIC SOLUTION; OTHER APPROACHES AND INSTRUMENTAL ANALYSIS; REFERENCES; CHAPTER 6. Determination of 1,3-Dienes: Diels-Alder Addition Methods; DETERMINATION OF ACYCLIC COMPOUNDS USING MALEIC ANHYDRIDE; DETERMINATION OF ANTHRACENE
- DETERMINATION OF CYCLOPENTADIENEGENERAL METHODS FOR 1,3-DIENES; INSTRUMENTAL ANALYSIS AND SEPARATIONS; REFERENCES; CHAPTER 7. Determination of Electron-rich Compounds: Electron-Donor-Acceptor Complexes and Charge Transfer Spectra; STABILITY OF THE COMPLEXES; CHARGE TRANSFER SPECTRA; CHARACTERIZATION OF ELECTRON DONORS; DETERMINATION OF ELECTRON DONORS; OXIDATION WITH ELECTRON ACCEPTORS; INSTRUMENTAL ANALYSIS AND SEPARATIONS; REFERENCES; PART II:; Author's note; CHAPTER 1. The Determination of Aldehydes in Oil of Lemon
- CHAPTER 2. The Estimation of Aldehydes and Ketones by Means of HydroxylamineCHAPTER 3. Improved Hydroxylamine Method for the Determination of Aldehydes and Ketones Displacement of Oxime Equilibria by Means of Pyridine; ANALYTICAL RESULTS; REFERENCES; CHAPTER 4. Determination of Carbonyl Compounds; REAGENTS; PROCEDURE; DEVELOPMENT OF METHOD; REFERENCES; CHAPTER 5. Macro- and Semimicrodetermination of Aldehydes and Ketones by Reaction with Hydroxylammonium Formate; MODIFIED MACRO METHOD; REFERENCES; CHAPTER 6.Studies on the Mechanism of Oxime and Semicarbazone Formationa; RESULTS; DISCUSSION