Cargando…
Selective sample handling and detection in high-performance liquid chromatography. Part B /
This is the second of a two-volume project which treats the handling, separation and detection of complex samples as an integrated, interconnected process. On the basis of this philosophy the editors have selected those contributions which demonstrate that optimal sample preparation leads to a simpl...
| Clasificación: | Libro Electrónico |
|---|---|
| Otros Autores: | , |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Amsterdam ; New York :
Elsevier,
1989.
|
| Colección: | Journal of chromatography library ;
v. 39B. |
| Temas: | |
| Acceso en línea: | Texto completo Texto completo |
Tabla de Contenidos:
- Front Cover; Selective Sample Handling and Detection in High-Performance Liquid Chromatography; Copyright Page; Contents; List of Contributors; Preface; CHAPTER I. PRECONCENTRATION AND CHROMATOGRAPHY ON CHEMICALLY MODIFIED SILICAS WITH COMPLEXATION PROPERTIES; 1. Introduction; 2. Chemically modified silicas; 3. Preconcentration of inorganic compounds using chelating silicas; 4. The preconcentration of organic compounds using chelating silicas; 5. Chelating silicas in chromatography; 6. Conclusion; References; CHAPTER II. SAMPLE HANDLING IN ION CHROMATOGRAPHY; 1. Introduction
- 2. Sample collection and dissolution3. Sample cleanup methods; 4. Contamination effects; 5. Sample handling for ultra-trace analysis; 6. Matrix elimination methods; 7. Conclusion; References; CHAPTER III. WHOLE BLOOD SAMPLE CLEAN-UP FOR CHROMATOGRAPHIC ANALYSIS; 1. Introduction; 2. Extraction procedures for blood samples; 3. Blood-sample preparation and HPCL analysis of SandimmunR (cyclosporine); 4. Trouble shooting in development of blood-sample clean-up; References; CHAPTER IV. RADIO-COLUMN LIQUID CHROMATOGRAPHY; 1. Introduction
- 2. Principles of scintillation counting in column liquid chromatography3. Optimization parameters for flow-through �-counting; 4. Applications; 5. Concluding remarks; References; CHAPTER V. MODERN POST-COLUMN REACTION DETECTION IN HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY; 1. General introduction; 2. Types of post-column reactors; 3. Choice of reaction detector; 4. Applications of post-column reaction detection; 5. New approaches to post-column Reaction Detection; 6. Conclusions; References; CHAPTER VI. NEW LUMINESCENCE DETECTION TECHNIQUES; 1. Introduction
- 2. Chemiluminescence detection with solid state reactors3. Liquid phase phosphorescence detection; References; CHAPTER VII. CONTINUOUS SEPARATION TECHNIQUES IN FLOW-INJECTION ANALYSIS; 1. Introduction; 2. Gas-liquid interfaces; 3. Gas-solid interfaces; 4. Liquid-liquid interfaces; 5. Solid-liquid interfaces; 6. HPLC-FIA association; 7. Final remarks; References; Subject Index; Journal of Chromatography Library (other volumes in the series)