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Separation methods in drug synthesis and purification /
Separation Methods in Drug Synthesis and Purification.
| Clasificación: | Libro Electrónico |
|---|---|
| Otros Autores: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Amsterdam ; New York :
Elsevier,
2000.
|
| Colección: | Handbook of analytical separations ;
v. 1. |
| Temas: | |
| Acceso en línea: | Texto completo Texto completo Texto completo |
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| 245 | 0 | 0 | |a Separation methods in drug synthesis and purification / |c edited by Kl�ara Valk�o. |
| 260 | |a Amsterdam ; |a New York : |b Elsevier, |c 2000. | ||
| 300 | |a 1 online resource (xxi, 589 pages) : |b illustrations | ||
| 336 | |a text |b txt |2 rdacontent | ||
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| 490 | 1 | |a Handbook of analytical separations ; |v v. 1 | |
| 504 | |a Includes bibliographical references and index. | ||
| 588 | 0 | |a Print version record. | |
| 506 | |3 Use copy |f Restrictions unspecified |2 star |5 MiAaHDL | ||
| 533 | |a Electronic reproduction. |b [Place of publication not identified] : |c HathiTrust Digital Library, |d 2010. |5 MiAaHDL | ||
| 538 | |a Master and use copy. Digital master created according to Benchmark for Faithful Digital Reproductions of Monographs and Serials, Version 1. Digital Library Federation, December 2002. |u http://purl.oclc.org/DLF/benchrepro0212 |5 MiAaHDL | ||
| 583 | 1 | |a digitized |c 2010 |h HathiTrust Digital Library |l committed to preserve |2 pda |5 MiAaHDL | |
| 505 | 0 | |a Front Cover -- Separation Methods in Drug Synthesis and Purification -- Copyright Page -- Contents -- Editor's Preface -- Series Editor's Preface -- List of Contributors -- Chapter 1. Comparison of various modes and phase systems for analytical HPLC -- 1.1 Fundamentals of HPLC -- 1.2 Chromatographic column and column packing particles -- 1.3 Separation modes in HPLC -- 1.4 Method development and optimisation of conditions in isocratic HPLC -- 1.5 Development of gradient-elution separations -- 1.6 Acknowledgements -- 1.7 References -- Chapter 2. Fast generic HPLC methods -- 2.1 Introduction. | |
| 505 | 8 | |a 2.2 Theory -- 2.3 Strategy for production of fast gradients -- 2.4 Fast gradients in practice -- 2.5 References -- Chapter 3. Application of standard methods in capillary electrophoresis for drug analysis -- 3.1 Introduction to capillary electrophoresis -- 3.2 Analysis of pharmaceuticals by CE -- 3.3 Low-pH buffer for analysis of basic drugs -- 3.4 High-pH buffer for analysis of acidic drugs -- 3.5 Micellar electrokinetic chromatography (MEKC) for neutral and/or charged drugs -- 3.6 Microemulsion electrokinetic chromatography (MEEKC) for neutral and/or charged drugs. | |
| 505 | 8 | |a 3.7 Indirect UV detection method for analysis of inorganic anions -- 3.8 Indirect UV detection method for analysis of simple organic acids -- 3.9 Indirect UV detection method for analysis of metal ions -- 3.10 Non-aqueous CE for analysis of acidic and basic drugs -- 3.11 Benefits of adopting standard CE methods -- 3.12 References -- Chapter 4. Capillary electrochromatography (CEC) -- 4.1 Introduction -- 4.2 Basic principles of capillary electrochromatography -- 4.3 Mobile phase composition -- 4.4 Stationary phases used in CEC -- 4.5 Operational characteristics of CEC. | |
| 505 | 8 | |a 4.6 Gradient and pressure-assisted (pseudo) CEC -- 4.7 Conclusions -- 4.8 Glossary of symbols -- 4.9 References -- Chapter 5. Coupled chromatography-mass spectrometry techniques for the analysis of combinatorial libraries -- 5.1 Introduction -- 5.2 LC/MS analysis of high-throughput parallel synthesis libraries -- 5.3 Example for monitoring the rehearsal phase of the synthesis of a solid-phase library -- 5.4 LC/UV/MS as a pre-screen for autoprep-solution phase -- 5.5 Assisted automated LC/MS analysis -- 5.6 The analysis of split-pool combinatorial libraries -- 5.7 Conclusions and future. | |
| 505 | 8 | |a 5.8 References -- Chapter 6. Optimization strategies for HPLC and CZE -- 6.1 Introduction -- 6.2 Responses and response functions -- 6.3 Univariate optimization strategies -- 6.4 Factorial methods -- 6.5 Mixture designs -- 6.6 Robustness/ruggedness -- 6.7 The simplex sequential approach -- 6.8 Automating the whole process: expert systems and knowledge based systems -- 6.9 References -- Chapter 7. Strategies for the development of process chromatography as a unit operation for the pharmaceutical industry -- 7.1 Introduction -- 7.2 The process development cycle. | |
| 520 | |a Separation Methods in Drug Synthesis and Purification. | ||
| 650 | 0 | |a Drugs |x Analysis. | |
| 650 | 0 | |a Drug development. | |
| 650 | 0 | |a Separation (Technology) | |
| 650 | 0 | |a Pharmaceutical chemistry. | |
| 650 | 1 | 2 | |a Chemistry, Pharmaceutical |x methods |0 (DNLM)D002626Q000379 |
| 650 | 2 | 2 | |a Chemistry, Analytical |x methods |
| 650 | 2 | 2 | |a Pharmaceutical Preparations |x isolation & purification |0 (DNLM)D004364Q000302 |
| 650 | 2 | |a Chemistry, Pharmaceutical |0 (DNLM)D002626 | |
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| 650 | 6 | |a M�edicaments |x D�eveloppement. |0 (CaQQLa)201-0306620 | |
| 650 | 6 | |a S�eparation (Technologie) |0 (CaQQLa)201-0000375 | |
| 650 | 6 | |a Chimie pharmaceutique. |0 (CaQQLa)201-0028674 | |
| 650 | 7 | |a MEDICAL |x Drug Guides. |2 bisacsh | |
| 650 | 7 | |a MEDICAL |x Pharmacology. |2 bisacsh | |
| 650 | 7 | |a MEDICAL |x Pharmacy. |2 bisacsh | |
| 650 | 7 | |a MEDICAL |x Nursing |x Pharmacology. |2 bisacsh | |
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| 650 | 7 | |a Drugs |x Analysis |2 fast |0 (OCoLC)fst00898769 | |
| 650 | 7 | |a Pharmaceutical chemistry |2 fast |0 (OCoLC)fst01060115 | |
| 650 | 7 | |a Separation (Technology) |2 fast |0 (OCoLC)fst01112723 | |
| 655 | 4 | |a Internet Resources. | |
| 700 | 1 | |a Valk�o, Kl�ara. | |
| 776 | 0 | 8 | |i Print version: |t Separation methods in drug synthesis and purification. |d Amsterdam ; New York : Elsevier, 2000 |z 0444500073 |z 9780444500076 |w (OCoLC)45486148 |
| 830 | 0 | |a Handbook of analytical separations ; |v v. 1. | |
| 856 | 4 | 0 | |u https://sciencedirect.uam.elogim.com/science/book/9780444500076 |z Texto completo |
| 856 | 4 | 0 | |u https://sciencedirect.uam.elogim.com/science/handbooks/15677192/1 |z Texto completo |
| 856 | 4 | 0 | |u https://sciencedirect.uam.elogim.com/science/bookseries/15677192/1 |z Texto completo |