Cargando…
Chemical projects scale up : how to go from laboratory to commercial /
Chemical Projects Scale Up: How to Go from Laboratory to Commercial covers the chemical engineering steps necessary for taking a laboratory development into the commercial world. The book includes the problems associated with scale up, equipment sizing considerations, thermal characteristics associa...
| Clasificación: | Libro Electrónico |
|---|---|
| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Amsterdam, Netherlands :
Elsevier,
[2018]
|
| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- Cover; Title Page; Copyright Page; Contents; Introduction; 1
- Potential Problems With Scale-up; Equipment Related; Mode Related; Theoretical Considerations; Thermal Characteristics; Safety Considerations; Recycle Considerations; Regulatory Requirements; Project Focus Considerations; Take Home Message; 2
- Equipment Design Considerations; Introduction; Reactor Scale-up; Laboratory Batch Reactor to Larger Batch Reactor (Pilot Plant or Commercial); Laboratory Batch Reactor to a Commercial Continuous Stirred Tank Reactor; Laboratory Batch Reactor to a Commercial Tubular Reactor
- Laboratory Tubular Reactor to a Commercial Tubular ReactorReactor Scale-up Example; Problem 2-1; Summary of Considerations for Reactor Scale-up; Supplier's Scale-ups; Volatile Removal Scale-up; Example Problem 2-2; Problem Statement; Summary of Key Points for Scale-up of Volatiles Removal Equipment; Other Scale-ups Using the Same Techniques; Solid-Liquid Separation; Example Problem 2-3; Problem Statement; Given; Pilot Plant Data; Required Commercial Operating Needs; Problem Approach; Pilot Plant Calculations and Comments; Commercial Calculations; 3
- Developing Commercial Process Flow Sheets
- 4
- Thermal Characteristics for Reactor Scale-up5
- Safety Considerations; Use of New Chemicals; Change in Delivery Mode for Chemicals; Impact of a New Development on Shared Facilities; Reaction By-Products That Might be Produced; Storage and Shipping Considerations; Step-Out Designs; 6
- Recycle Considerations; Why Have a Recycle System in a Pilot Plant?; Impurity Buildup Considerations; 7
- Supplier's Equipment Scale-up; Agitator and Mixer Scale-up; Indirect Heated Dryer; Summary of Working With Suppliers of Specialty Equipment; 8
- Sustainability; Long-Term Changes in Existing Technology
- Long-Term Availability and Cost of Feeds and CatalystsLong-Term Availability and Cost of Utilities; Disposition of Waste and By-Product Streams; Operability and Maintainability of Process Facilities; Summary; 9
- Project Evaluation Using CAPEX and OPEX Inputs; Introduction; CAPEX and OPEX; Project Timing and Early Design Calculations; 10
- Emerging Technology Contingency (ETC); Application; Contributors/Reviewers; References; 11
- Other Uses of Study Designs; Identifying High Cost Parts of CAPEX and OPEX; Identifying Areas Where Unusual or Special Equipment Is Required
- Identifying Areas for Future Development WorkIdentifying the Size-limiting Equipment; Identifying Areas Where There Is a Need for Consultants; Summary; 12
- Scaling Up to Larger Commercial Sizes; Summary; 13
- Defining and Mitigating Risks; Techniques for Definition and Mitigation of Risk; Required Manpower Resources; Reasonable Schedules; Cooperative Team Spirit and Culture; 14
- Typical Cases Studies; Successful Case Studies; Unsuccessful Case Studies; Production of an Inorganic Catalyst; Development of a New Polymerization Platform.