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Basics of Polymers, Volume II : Instrumental Methods of Testing /
Wide-range polymer materials require polymer testing, which is associated with public and economic factors. Perhaps in no other aspect of the materials is there a great need for a dispassionate and rigorous analysis because of the characteristics of a polymer. Polymer testing with instrumental metho...
| Clasificación: | Libro Electrónico |
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| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
[Place of publication not identified] :
Momentum Press,
2019.
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| Temas: | |
| Acceso en línea: | Texto completo |
MARC
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| 100 | 1 | |a Muralisrinivasan, Subramanian, |e author. | |
| 245 | 1 | 0 | |a Basics of Polymers, Volume II : |b Instrumental Methods of Testing / |c Subramanian Muralisrinivasan. |
| 264 | 1 | |a [Place of publication not identified] : |b Momentum Press, |c 2019. | |
| 300 | |a 1 online resource | ||
| 336 | |a text |b txt |2 rdacontent | ||
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| 505 | 0 | |a 1. Introduction -- 1.1. Objective: polymer testing -- 1.2. Necessity of instrumental methods -- 1.3. Specialization | |
| 505 | 8 | |a 2. Importance of polymer testing -- 2.1. Polymers -- 2.1.1. Chemical aspects -- 2.1.2. Architectural aspects -- 2.2. Polymer properties -- 2.3. Functionality type distribution -- 2.4. Chemical composition distribution -- 2.5. Physical properties -- 2.6. Chemical properties -- 2.7. Thermal properties -- 2.8. Rheological properties -- 2.9. Additives -- 2.10. Testing of additives -- 2.11. Instrumental methods and their role -- 2.12. Spectroscopy -- 2.13. Chromatography -- 2.14. Thermal analysis -- 2.15. Rheological measurements -- 2.16. Other measurements -- 2.17. Chemical methods versus instrumental methods -- 2.18. Importance of instrumental methods | |
| 505 | 8 | |a 3. Spectroscopic techniques -- 3.1. Spectrophotometric analysis -- 3.2. Fourier transform -- 3.3. Ultraviolet and visible absorption spectroscopy -- 3.4. Near-infrared (NIR) spectroscopy -- 3.4.1. Industrial applications -- 3.4.2. Advantages -- 3.4.3. Disadvantage -- 3.5. Infrared spectroscopy -- 3.5.1. Basics -- 3.5.2. Fourier transform infrared spectrophotometer -- 3.5.3. Instrumentation -- 3.5.4. Interferometry -- 3.5.5. Attenuated total reflectance -- 3.5.6. Importance of infrared spectroscopy -- 3.5.7. Identification of unknown compounds -- 3.5.8. Elemental analysis -- 3.5.9. Quantitative analysis -- 3.5.10. Molecular structure -- 3.5.11. Infrared spectrum -- 3.5.12. Shortcomings -- 3.5.13. Some of the advantages of FTIR are -- 3.6. Mass spectrometry -- 3.6.1. Instrumentation -- 3.6.2. Mass spectrometry and polymers -- 3.6.3. Pyrolysis-mass spectrometry -- 3.6.4. Secondary ion mass spectrometry -- 3.6.5. Electrospray ionization -- 3.6.6. Field desorption mass spectrometry 43 3.6.7. matrix-assisted laser desorption ionization time-of-flight 43 3.6.8. shortcomings -- 3.6.9. Advantages -- 3.7. Nuclear magnetic resonance spectroscopy -- 3.7.1. Basics -- 3.7.2. NMR spectrum -- 3.7.3. Solvents -- 3.7.4. Proton 1H NMR spectrum -- 3.7.5. Carbon 13C NMR spectrum -- 3.7.6. Fluorine 19F NMR spectrum -- 3.7.7. Shortcomings -- 3.7.8. Advantages -- 3.8. Raman spectroscopy -- 3.8.1. Importance of the raman spectrum -- 3.8.2. Shortcomings -- 3.8.3. Advantages | |
| 505 | 8 | |a 4. Chromatographic techniques -- 4.1. High-performance liquid chromatography -- 4.1.1. Instrumentation -- 4.1.2. Reverse phase HPLC -- 4.1.3. Mobile phase -- 4.1.4. Stationary phase -- 4.1.5. Elution -- 4.1.6. Column -- 4.1.7. Mechanism of retention -- 4.1.8. Chromatogram -- 4.1.9. Advantages -- 4.1.10. Shortcomings -- 4.2. Size exclusion chromatography -- 4.2.1. Instrumentation -- 4.2.2. Detectors -- 4.2.3 Effects on column packing -- 4.2.4. Effects on velocity -- 4.2.5. Solvents effect -- 4.2.6. Calibration -- 4.2.7. Plate count -- 4.2.8. Role of SEC -- 4.2.9. Shortcomings -- 4.2.10. Advantages -- 4.3. Gas chromatography -- 4.3.1. Thermal fragmentation -- 4.3.2. Instrumentation -- 4.3.3. Analyte separation and quantitative determination -- 4.3.4. Shortcomings -- 4.3.5. Advantages | |
| 505 | 8 | |a 5. Thermal analysis -- 5.1. Thermogravimetric analysis (TGA) -- 5.1.1. Importance of thermal analysis -- 5.1.2. Instrumentation -- 5.1.3. Essentials of thermogravimetric instrument -- 5.1.4. Advantages -- 5.2. Differential scanning calorimetry (DSC) -- 5.2.1. Basics -- 5.2.2. Instrumentation -- 5.2.3. Advantages | |
| 505 | 8 | |a 6. Other essential instrumental methods of analysis -- 6.1. Heat stability test -- 6.2. Gel content determination -- 6.3. Microscopy -- 6.4. Scanning electron microscopy -- 6.5. Transmission electron microscopy (TEM) -- 6.6. Atomic force microscopy (AFM) -- 6.7. Small-angle x-ray scattering (SAXS) -- 6.8. Viscometric determination of molecular weight -- 6.9. Ultracentrifugation -- 6.10. Light scattering technique -- 6.11. Supercritical fluid extraction (SFE) -- 6.11.1. Advantages | |
| 505 | 8 | |a 7. Future trends -- 7.1. Role of polymer testing -- 7.2. Quality control -- 7.3. Developments in polymer testing -- 7.4. Driving forces -- 7.5. Requirements and challenges | |
| 505 | 8 | |a About the author -- Index. | |
| 520 | 3 | |a Wide-range polymer materials require polymer testing, which is associated with public and economic factors. Perhaps in no other aspect of the materials is there a great need for a dispassionate and rigorous analysis because of the characteristics of a polymer. Polymer testing with instrumental methods are reliable with respect to technological options and economics of the operations. Polymer testing is long established and highly successful. However, the variations in the raw materials and additives, yet not without particular problems such as variations in molecular weight, result in quality problems in the product. | |
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