Gas chromatography and mass spectrometry : a practical guide /

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Gas Chromatography and Mass Spectrometry: A Practical Guide is the second edition to the highly successful book of the same name, originally written by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996). Designed as a valuable resource to the GC/MS user, this book provides serves as a one-stop-shop co...

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Detalles Bibliográficos
Clasificación:Libro Electrónico
Autor principal: Sparkman, O. David (Orrin David), 1942-
Otros Autores: Penton, Zelda, Kitson, Fulton G.
Formato: Electrónico eBook
Idioma:Inglés
Publicado: Burlington, MA : Academic Press, 2011.
Edición:2nd ed.
Temas:
Gas chromatography.
Mass spectrometry.
Chromatography, Gas
Mass Spectrometry
Chromatographie en phase gazeuse.
Spectrométrie de masse.
gas chromatography.
mass spectrometry.
SCIENCE > Chemistry > Analytic.
Gaschromatographie
Massenspektrometrie
GC-MS
Spektrografi.
Acceso en línea:Texto completo
Tabla de Contenidos:
  • The fundamentals of GC/MS
  • Introduction and history
  • Gas chromatography
  • The GC/MS interface
  • Mass spectrometry instrumentation
  • Mass spectral data interpretation
  • Quantitation with GC/MS
  • GC conditions, derivatization, and mass spectral interpretation of specific compound types
  • Acids
  • Alcohols
  • Aldehydes
  • Amides
  • Amines
  • Amino acids
  • Common contaminants
  • Drugs and their metabolites
  • Esters
  • Ethers
  • Fluorinated compounds
  • Gases
  • Glycols
  • Halogenated compounds (other than fluorinated compunds)
  • Hydrocarbons
  • Isocyanates
  • Ketones
  • Nitriles
  • Nitroaromatics
  • Nitrogen-containing heterocyclic compunds
  • Nucleosides (TMS derivatives)
  • Pesticides
  • Phenols
  • Phosphorus compounds
  • Plasticizers and other polymer additives (including phthalates)
  • Prostaglandins (MO-TMS derivatives)
  • Solvents and their impurities
  • Steroids
  • Sugars (monosaccharides)
  • Sulfur compounds
  • Appendices
  • A definitions of terms related to gas chromatography
  • B definitions of terms related to mass spectrometry
  • C atomic masses and isotope abundances and other information for the determination of an elemental composition from isotope peak intensity rations
  • X+1 and x+2 values for ions containing atoms of C and H based on isotope contributions
  • E isotope peak patterns for ions containing atoms of Cl and/or Br
  • F steps to follow in the determination of an elemental composition based on isotope peak intensity ratios
  • G derivatization in GC/MS
  • H points of comparison of LC/MS vs GC/MS
  • I list of available EI mass spectral databases
  • J information required for reporting a GC/MS analysis
  • K third-party software for use with GC/MS
  • L GC installation and maintenance
  • M Troubleshooting common GC problems
  • N maintenance, operating tips, and troubleshooting for mass spectrometers
  • O mixtures for determining mass spectral resolution
  • P cross-index chart for GC stationary phases
  • Q ions for determining unknown structures.

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