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Differentiation of chiral compounds using NMR spectroscopy /
Differentiation of Chiral Compounds Using NMR Spectroscopy offers a thoroughly revised second edition to the essential volume that puts the focus on the chiral systems that are commercially available and have been widely vetted for use in NMR spectroscopy. The text covers a broad range of reagents t...
| Clasificación: | Libro Electrónico |
|---|---|
| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Hoboken, NJ :
John Wiley & Sons, Inc.,
2018.
|
| Edición: | Second edition. |
| Temas: | |
| Acceso en línea: | Texto completo |
MARC
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| 100 | 1 | |a Wenzel, Thomas J., |e author. | |
| 245 | 1 | 0 | |a Differentiation of chiral compounds using NMR spectroscopy / |c Thomas J. Wenzel. |
| 250 | |a Second edition. | ||
| 264 | 1 | |a Hoboken, NJ : |b John Wiley & Sons, Inc., |c 2018. | |
| 264 | 4 | |c ©2018 | |
| 300 | |a 1 online resource (xxi, 584 pages) | ||
| 336 | |a text |b txt |2 rdacontent | ||
| 337 | |a computer |b c |2 rdamedia | ||
| 338 | |a online resource |b cr |2 rdacarrier | ||
| 504 | |a Includes bibliographical references and index. | ||
| 588 | 0 | |a Online resource; title from digital title page (viewed on July 02, 2018). | |
| 505 | 0 | |a Introduction -- Aryl-containing carboxylic acids -- Other carboxylic acid-based reagents -- Hydroxyl- and thiol-containing reagents -- Amine-based reagents -- Miscellaneous CDAS, CSAS, and other methods of chiral analysis -- Reagents incorporating phosphorus, selenium, boron, and silicon atoms -- Macrocyclic and receptor compounds as chiral nmr differentiating agents -- Chiral differentiation with metal-based reagents -- Chiral NMR differentiation using ordered systems -- Closing comments and future prospects. | |
| 520 | |a Differentiation of Chiral Compounds Using NMR Spectroscopy offers a thoroughly revised second edition to the essential volume that puts the focus on the chiral systems that are commercially available and have been widely vetted for use in NMR spectroscopy. The text covers a broad range of reagents that make it possible to determine the enantiomeric purity and assign the absolute configuration of many classes of compounds. Comprehensive in scope, the text describes the chiral NMR differentiating agents as derivatizing agents, solvating agents, metal-based reagents and liquid crystals and gels, and explains the range and types of compounds for which they can be used for analysis. New to this edition are the most recent findings in the field as well as the development of advanced NMR measurement techniques that allow for the simplification of complex spectra resulting in more readily identified enantiodifferentiation.--Provided by publisher. | ||
| 590 | |a ProQuest Ebook Central |b Ebook Central Academic Complete | ||
| 650 | 0 | |a Chemical tests and reagents. | |
| 650 | 0 | |a Nuclear magnetic resonance spectroscopy. | |
| 650 | 0 | |a Chirality. | |
| 650 | 2 | |a Magnetic Resonance Spectroscopy | |
| 650 | 6 | |a Chimie |x Essais et réactifs. | |
| 650 | 6 | |a Spectroscopie de la résonance magnétique nucléaire. | |
| 650 | 6 | |a Chiralité. | |
| 650 | 7 | |a SCIENCE |x Chemistry |x Analytic. |2 bisacsh | |
| 650 | 7 | |a Chemical tests and reagents |2 fast | |
| 650 | 7 | |a Chirality |2 fast | |
| 650 | 7 | |a Nuclear magnetic resonance spectroscopy |2 fast | |
| 758 | |i has work: |a Differentiation of chiral compounds using NMR spectroscopy (Text) |1 https://id.oclc.org/worldcat/entity/E39PCYhCq4hcWBpFCWWqkk7Dmb |4 https://id.oclc.org/worldcat/ontology/hasWork | ||
| 776 | 0 | 8 | |i Print version: |a Wenzel, Thomas J. |t Differentiation of chiral compounds using NMR spectroscopy. |b Second edition. |d Hoboken, NJ : John Wiley & Sons, 2018 |z 9781119323914 |w (DLC) 2018003400 |
| 856 | 4 | 0 | |u https://ebookcentral.uam.elogim.com/lib/uam-ebooks/detail.action?docID=5407778 |z Texto completo |
| 880 | 0 | |6 505-00/(S |a and 2-Fluoro-2-(2-Naphthyl)Propionic Acid 59 2.16 α-Methoxy-α-(1-Naphthyl)Acetic Acid/α-Methoxy-α-(2-Naphthyl)Acetic Acid 61 2.17 2-tert-Butoxy-2-(2-Naphthyl)Acetic Acid (2-NTBA) 62 2.18 (−)-(R)-(2-Naphthyloxy)Phenylacetic Acid 63 2.19 α-Methoxy-α-Trifluoromethyl-1-Naphthylacetic Acid (MTN(1)A) 63 2.20 Naproxen 64 2.21 2-Methoxy-2-(1-Naphthyl)Propionic Acid (MαNP) 65 2.22 O-Aryl Lactic Acids 70 2.23 α-(2-Anthryl)-α-Methoxyacetic Acid (2-AMA)/α-(9-Anthryl)-α-Methoxyacetic Acid (9-AMA) 72 2.24 Summary 75 3. | |
| 880 | 0 | |6 505-00/(S |a Self-Differentiation of Chiral Compounds 234 6.20 High-Throughput Methods with Chiral NMR Reagents 236 6.21 HPLC-NMR 237 6.22 Database Methods 238 7. Reagents Incorporating Phosphorus, Selenium, Boron, and Silicon Atoms 243 7.1 Phosphorus-Containing Reagents 243 7.2 Selenium-Containing Reagents 282 7.3 Boron-Containing Reagents 285 7.4 Silicon-Containing Reagents 294 8. Macrocyclic and Receptor Compounds as Chiral NMR Differentiating Agents 297 8.1 Cyclodextrins 298 8.2 Crown Ethers 322 8.3 Calixarenes and Resorcinarenes 345 8.4 Receptor Compounds 360 8.5 Cyclosophoraoses: Cyclic-β-d-Glucans 366 8.6 Cryptophane Receptor 367 8.7 1, 1′-Binaphthalene-Based Macrocycles and Receptors 369 9. | |
| 880 | 0 | |6 505-00/(S |a Other Carboxylic Acid-Based Reagents 79 3.1 Camphanic Acid 79 3.2 Menthoxyacetic Acid 81 3.3 Tetra-tert-Butyltrioxabicyclo[3.3.1-Nonadienedicarboxylic Acid 82 3.4 Di-O-Benzoyl Tartaric Acid/Di-O-p-Toluoyl Tartaric Acid 82 3.5 2-(2, 3-Anthracenedicarboximido)Cyclohexane Carboxylic Acid 85 3.6 3β-Acetoxy-Δ5-Etiocholenic Acid 87 3.7 1-Methoxy-2, 3-Dihydro-1H-Cyclopenta[a-Naphthalene-1-Carboxylic Acid 88 3.8 1-Fluoroindan-1-Carboxylic Acid 88 3.9 (−)-(R)-2-(2, 3, 4, 5, 6-Pentafluorophenoxy)-2-(Phenyl-d5)Acetic Acid 89 3.10 2, 2-Diphenyl- and 2, 2-Di-2-Naphthalen-2-yl-[1, 3-Dioxolane-4, | |
| 880 | 0 | |6 505-00/(S |a Aryl-Containing Carboxylic Acids 19 2.1 Introduction 19 2.2 α-Methoxy-α-Trifluoromethylphenylacetic Acid (Mosher's Reagent) 22 2.3 α-Methoxy-α-Trifluoromethylphenylacetic Thioacid 35 2.4 α-Methoxyphenylacetic Acid 35 2.5 Mandelic Acid (2-Hydroxy-2-Phenylacetic Acid) 47 2.6 O-Acetyl Mandelic Acid (2-Acetoxy-2-Phenylacetic Acid) 49 2.7 Other O-Derivatized Mandelic Acids 51 2.8 2-Phenylpropionic Acid 52 2.9 2-Phenylselenopropionic Acid 52 2.10 2-Methoxy-2-Phenylpent-3-ynoic Acid 52 2.11 3-Phenylbutanoic Acid/2-Phenylbutanoic Acid 53 2.12 α-Cyano-α-Fluorophenylacetic Acid/α-Cyano-α-Fluoronaphthylacetic Acid/α-Cyano-α-Fluorop-Tolylacetic Acid 54 2.13 N-Boc Phenylglycine (BPG) 56 2.14 1, 5-Difuoro-2, 4-Dinitrobenzene and Derivatives 57 2.15 2-Fluoro-2-Phenylacetic Acid, 2-Fluoro-2-(1-Naphthyl) Propionic Acid, | |
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