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170121s2016 xx ob 001 0 eng d |
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|a 9781118929131
|b Wiley
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|a QD411.7.S94.R545 2017
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|a 547.05045299999995
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|a UAMI
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|a Rieke, Reuben D.
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|a Chemical Synthesis Using Highly Reactive Metals.
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|a Somerset :
|b John Wiley & Sons, Incorporated,
|c 2016.
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| 300 |
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|a 1 online resource (483 pages)
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| 336 |
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|a text
|b txt
|2 rdacontent
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|a computer
|b c
|2 rdamedia
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|a online resource
|b cr
|2 rdacarrier
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|a Print version record.
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|6 880-01
|a Title Page ; Copyright Page; Contents; Preface; Chapter 1 Genesis of Highly Reactive Metals ; Chapter 2 General Methods of Preparation and Properties ; 2.1 General Methods for€Preparation of€Highly Reactive Metals; 2.2 Physical Characteristics of€Highly Reactive Metal€Powders; 2.3 Origin of€the€Metals' High Reactivity; References; Chapter 3 Zinc ; 3.1 General Methods for€Preparation of€Rieke Zinc; 3.2 Direct Oxidative Addition of€Reactive Zinc to€Functionalized Alkyl, Aryl, and€Vinyl Halides; Typical Preparation of 3-Fluorobenzylzinc Bromide ; Typical Preparation of 4-Cyanobutylzinc Bromide.
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|a 3.7 Intramolecular Cyclizations and€Conjugate Additions Mediated by Rieke Zinc3.8 The Formation and€Chemistry of€Secondary and€Tertiary Alkylzinc Halides; 3.9 Electrophilic Amination of€Organozinc Halides; 3.10 Reformatsky and Reformatsky-Like Reagents and Their Chemistry ; Synthesis of€Reformatsky Reagent in€THF; Synthesis of€Reformatsky Reagent in€Diethyl Ether; 3.11 Configurationally Stable Organozinc Reagents and€Intramolecular Insertion Reactions; 3.12 Preparation of€Tertiary Amides via Aryl, Heteroaryl, and€Benzyl Organozinc Reagents; 3.13 Preparation of 5-Substituted-2-Furaldehydes.
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|a Results and€DiscussionGeneral Procedure for Pd-Catalyzed Cross-Coupling Reactions ; 3.14 Preparation and Chemistry of 4-Coumarylzinc Bromide ; 3.15 Preparation and Cross-Coupling of 2-Pyridyl and 3-Pyridylzinc Bromides ; Results and€Discussion; Conclusions; Experimental; General; Preparation of 2-Pyridylzinc Bromide (P1) ; Preparation of 3-Pyridylzinc Bromide (P7) ; General Procedure for Copper-Free Coupling Reactions ; Pd-Catalyzed Coupling Reaction with 4-Iodoanisole (10b) ; Preparation of€Bipyridines; Pd-Catalyzed Coupling Reaction with Haloanilines.
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|a Pd-Catalyzed Coupling Reactions with Halophenols.
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|a Includes bibliographical references at the end of each chapters and index.
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| 590 |
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|a ProQuest Ebook Central
|b Ebook Central Academic Complete
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| 650 |
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|a Organometallic chemistry.
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| 650 |
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|a Chemical reactions.
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|a Metals.
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|a Metals
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|a Chimie organométallique.
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|a Métaux.
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|a metal.
|2 aat
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|a SCIENCE
|x Chemistry
|x Organic.
|2 bisacsh
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| 650 |
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|a Chemical reactions
|2 fast
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| 650 |
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|a Metals
|2 fast
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| 650 |
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|a Organometallic chemistry
|2 fast
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| 776 |
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|i Print version:
|a Rieke, Reuben D.
|t Chemical Synthesis Using Highly Reactive Metals.
|d Somerset : John Wiley & Sons, Incorporated, ©2016
|z 9781118929117
|
| 856 |
4 |
0 |
|u https://ebookcentral.uam.elogim.com/lib/uam-ebooks/detail.action?docID=4756760
|z Texto completo
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| 880 |
8 |
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|6 505-00/(S
|a Typical Preparation of 4-Bromophenylzinc Iodide Typical Preparation of 3-Methyl-2-Pyridlyzinc Bromide ; 3.3 Reactions of€Organozinc Reagents with Acid€Chlorides; Typical Generation of Organozinc Halides from Organic Halides and Active Zinc and Their Copper-Mediated Coupling with Acid Chlorides ; Synthesis of€4-Methoxy-2′-Thiomethylbenzophenone Using Tetrakis(triphenylphosphine)palladium(0) as€Catalyst ; Synthesis of Ethyl 7-(3,4-Difluorophenyl)-7-Oxoheptanoate Using Copper Iodide as Catalyst ; Cyanide-Based Rieke Zinc ; 3.4 Reactions of€Organozinc Reagents with α, β-Unsaturated Ketones.
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|6 505-01/(S
|a Typical Copper-Mediated Conjugate Addition Reaction of€Organozinc Halides to€α, β-Unsaturated Ketones 3.5 Reactions of€Organozinc Reagents with€Allylic and€Alkynyl Halides; Typical Reaction of€Organozinc Halides with€Allylic Halides; Preparation of 2,3-Di(p-Cyanobenzyl)-1,3-Butadiene Reaction ; 3.6 Negishi Cross-Coupling of Vinyl and Aryl Organozinc Halides ; Typical Procedure for€the€Reaction of€RZnX with€Aryl and€Vinyl Halides; Preparation of Aryl Ketones via Ni-Catalyzed Negishi Coupling Reactions ; Typical Reaction Procedure.
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|a ProQuest Ebook Central
|b EBLB
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