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Handbook of GC-MS : Fundamentals and Applications.
The only comprehensive reference on this popular and rapidly developing technique provides a detailed overview, ranging from fundamentals to applications, including a section on the evaluation of GC-MS analyses. As such, it covers all aspects, including the theory and principles, as well as a broad...
| Clasificación: | Libro Electrónico |
|---|---|
| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Hoboken :
Wiley,
2015.
|
| Edición: | 3rd ed. |
| Temas: | |
| Acceso en línea: | Texto completo |
MARC
| LEADER | 00000cam a2200000 i 4500 | ||
|---|---|---|---|
| 001 | EBOOKCENTRAL_ocn908520023 | ||
| 003 | OCoLC | ||
| 005 | 20240329122006.0 | ||
| 006 | m o d | ||
| 007 | cr |n||||||||| | ||
| 008 | 150509s2015 xx ob 001 0 eng d | ||
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| 020 | |a 9783527674336 | ||
| 020 | |a 3527674330 | ||
| 020 | |z 9783527334742 | ||
| 020 | |z 9783527674329 |q (ePub) | ||
| 020 | |z 9783527674312 |q (Mobi) | ||
| 020 | |z 9783527674305 |q (oBook) | ||
| 029 | 1 | |a DEBBG |b BV044072477 | |
| 035 | |a (OCoLC)908520023 | ||
| 050 | 4 | |a QD272.C44 H83 2015 | |
| 082 | 0 | 4 | |a 543/.85 |
| 049 | |a UAMI | ||
| 100 | 1 | |a Hübschmann, Hans-Joachim. | |
| 245 | 1 | 0 | |a Handbook of GC-MS : |b Fundamentals and Applications. |
| 250 | |a 3rd ed. | ||
| 260 | |a Hoboken : |b Wiley, |c 2015. | ||
| 300 | |a 1 online resource (882 pages) | ||
| 336 | |a text |b txt |2 rdacontent | ||
| 337 | |a computer |b c |2 rdamedia | ||
| 338 | |a online resource |b cr |2 rdacarrier | ||
| 588 | 0 | |a Print version record. | |
| 505 | 0 | |a Cover; Title Page; Copyright; Dedication; Contents; Foreword; Preface to the Third Edition; Chapter 1 Introduction; 1.1 The Historical Development of the GC-MS Technique; Chapter 2 Fundamentals; 2.1 Sample Preparation; 2.1.1 Solid Phase Extraction; 2.1.2 Solid Phase Microextraction; 2.1.3 Pressurized Liquid Extraction; 2.1.3.1 In-Cell Sample Preparation; 2.1.3.2 In-Cell Moisture Removal; 2.1.3.3 In-Cell Hydrocarbon Oxidation; 2.1.4 Online Liquid Chromatography Clean-Up; 2.1.5 Headspace Techniques; 2.1.5.1 Static Headspace Technique; 2.1.5.2 Dynamic Headspace Technique (Purge and Trap). | |
| 505 | 8 | |a 2.1.5.3 Coupling of Purge and Trap with GC-MS Systems2.1.5.4 Headspace versus Purge and Trap; 2.1.6 Adsorptive Enrichment and Thermal Desorption; 2.1.6.1 Sample Collection; 2.1.6.2 Calibration; 2.1.6.3 Desorption; 2.1.7 Pyrolysis; 2.1.7.1 Foil Pyrolysis; 2.1.7.2 Curie Point Pyrolysis; 2.1.7.3 Micro-furnace Pyrolysis; 2.1.8 Thermal Extraction (Outgassing); 2.1.9 QuEChERS Sample Preparation; 2.2 Gas Chromatography; 2.2.1 Sample Inlet Systems; 2.2.2 Carrier Gas Regulation; 2.2.2.1 Forward Pressure Regulation; 2.2.2.2 Back Pressure Regulation; 2.2.2.3 Carrier Gas Saving. | |
| 505 | 8 | |a 2.2.3 Injection Port Septa2.2.3.1 Septum Purge; 2.2.3.2 The MicroSeal Septum; 2.2.4 Injection Port Liner; 2.2.4.1 Split Injection; 2.2.4.2 Splitless Injection; 2.2.4.3 Liner Activity and Deactivation; 2.2.4.4 Liner Geometry; 2.2.5 Vaporizing Sample Injection Techniques; 2.2.5.1 Hot Needle Thermo Spray Injection Technique; 2.2.5.2 Cold Needle Liquid Band Injection Technique; 2.2.5.3 Filled Needle Injections; 2.2.5.4 Split Injection; 2.2.5.5 Splitless Injection (Total Sample Transfer); 2.2.5.6 Concurrent Solvent Recondensation; 2.2.5.7 Concurrent Backflush. | |
| 505 | 8 | |a 2.2.6 Temperature Programmable Injection Systems2.2.6.1 The PTV Cold Injection System; 2.2.6.2 The PTV Injection Procedures; 2.2.6.3 On-Column Injection; 2.2.6.4 PTV On-Column Injection; 2.2.6.5 Cryofocussing; 2.2.6.6 PTV Cryo-Enrichment; 2.2.7 Capillary Column Choice and Separation Optimization; 2.2.7.1 Sample Capacity; 2.2.7.2 Internal Diameter; 2.2.7.3 Film Thickness; 2.2.7.4 Column Length; 2.2.7.5 Setting the Carrier Gas Flow; 2.2.7.6 Properties of Column Phases; 2.2.7.7 Properties of Ionic Liquid Phases; 2.2.8 Chromatography Parameters; 2.2.8.1 The Chromatogram and Its Meaning. | |
| 505 | 8 | |a 2.2.8.2 Capacity Factor k'2.2.8.3 Chromatographic Resolution; 2.2.8.4 Factors Affecting the Resolution; 2.2.8.5 Maximum Sample Capacity; 2.2.8.6 Peak Symmetry; 2.2.8.7 Optimization of Carrier Gas Flow; 2.2.8.8 Effect of Oven Temperature Ramp Rate; 2.2.9 Fast Gas Chromatography Solutions; 2.2.9.1 Fast Chromatography; 2.2.9.2 Ultra-Fast Chromatography; 2.2.10 Multi-Dimensional Gas Chromatography; 2.2.10.1 Heart Cutting; 2.2.10.2 Comprehensive GC -- GC x GC; 2.2.10.3 Modulation; 2.2.10.4 Detection; 2.2.10.5 Data Handling; 2.2.10.6 Moving Capillary Stream Switching. | |
| 500 | |a 2.2.11 Classical Detectors for GC-MS Systems. | ||
| 520 | |a The only comprehensive reference on this popular and rapidly developing technique provides a detailed overview, ranging from fundamentals to applications, including a section on the evaluation of GC-MS analyses. As such, it covers all aspects, including the theory and principles, as well as a broad range of real-life examples taken from laboratories in environmental, food, pharmaceutical and clinical analysis. It also features a glossary of approximately 300 terms and a substance index that facilitates finding a specific application. For this new edition the work has been now extended to two. | ||
| 504 | |a Includes bibliographical references and index at the end of each chapters. | ||
| 590 | |a ProQuest Ebook Central |b Ebook Central Academic Complete | ||
| 650 | 0 | |a Gas chromatography. | |
| 650 | 0 | |a Mass spectrometry. | |
| 650 | 2 | |a Chromatography, Gas | |
| 650 | 2 | |a Mass Spectrometry | |
| 650 | 6 | |a Chromatographie en phase gazeuse. | |
| 650 | 6 | |a Spectrométrie de masse. | |
| 650 | 7 | |a gas chromatography. |2 aat | |
| 650 | 7 | |a mass spectrometry. |2 aat | |
| 650 | 7 | |a Gas chromatography |2 fast | |
| 650 | 7 | |a Mass spectrometry |2 fast | |
| 776 | 0 | 8 | |i Print version: |a Hübschmann, Hans-Joachim. |t Handbook of GC-MS : Fundamentals and Applications. |d Hoboken : Wiley, ©2015 |z 9783527334742 |
| 856 | 4 | 0 | |u https://ebookcentral.uam.elogim.com/lib/uam-ebooks/detail.action?docID=1896065 |z Texto completo |
| 936 | |a BATCHLOAD | ||
| 938 | |a ProQuest Ebook Central |b EBLB |n EBL1896065 | ||
| 994 | |a 92 |b IZTAP | ||