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EBOOKCENTRAL_ocn876592818 |
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|a 875819003
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|z (OCoLC)875819003
|z (OCoLC)900213162
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|z (OCoLC)958545452
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|a QD945
|b .L77 2013eb
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|a SCI
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|2 bisacsh
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|a 548
|2 23
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|a UAMI
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|a Luger, Peter,
|d 1943-
|e author.
|1 https://id.oclc.org/worldcat/entity/E39PBJhMfwJPcpgw688McjQg8C
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1 |
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|a Modern X-ray analysis on single crystals :
|b a practical guide /
|c by Peter Luger.
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250 |
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|a 2nd edition.
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|a Berlin ;
|a Boston :
|b Walter de Gruyter GmbH & Co. KG,
|c 2013.
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|a 1 online resource
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|a text
|b txt
|2 rdacontent
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|a computer
|b c
|2 rdamedia
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|a online resource
|b cr
|2 rdacarrier
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|a Includes index.
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|a Print version record.
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|a 1 Introduction; 1.1 Historical remarks; 1.2 The crystal lattice: Basic definitions; 1.2.1 Periodicity, lattice constants; 1.2.2 Lattice points, lattice planes, reciprocal lattice; 1.3 Sample structures; 2 Fundamental results of diffraction theory, X-radiation; 2.1 Electron density and related functions; 2.2 Diffraction conditions for single crystals; 2.3 X-rays; 2.3.1 Generation of X-rays; 2.3.2 Absorption; 2.3.3 Filters, monochromators; 2.3.4 X-ray tubes; 2.3.5 Synchrotron radiation; 3 Preliminary experiments; 3.1 Film methods; 3.1.1 The rotation method; 3.1.2 Zero level Weissenberg method.
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|a 3.1.3 Upper level Weissenberg -- normal beam and equi-inclination method3.1.4 Precession technique; 3.2 Practicing film techniques; 3.2.1 Choice of experimental conditions; 3.2.2 Rotation and Weissenberg photographs of KAMTRA and SUCROS; 4 Crystal symmetry; 4.1 Symmetry operations in a crystal lattice; 4.1.1 Introduction; 4.1.2 Basic symmetry operations; 4.1.3 Crystal classes and related coordinate systems; 4.1.4 Translational symmetry, lattice types and space groups; 4.2 Crystal symmetry and related intensity symmetry; 4.2.1 Representation of? and F as Fourier series.
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|a 4.2.2 Thermal motion, displacement parameters4.2.3 Intensity symmetry, asymmetric unit; 4.2.4 Systematic extinctions; 4.2.5 Quasicrystals; 4.3 Space group determination; 4.3.1 General considerations, practical aspects; 4.3.2 Space groups of KAMTRA and SUCROS from film exposures; 5 Diffractometer measurements; 5.1 Point detector data collection on a four-circle diffractometer; 5.1.1 Eulerian cradle geometry; 5.1.2 Choice of experimental conditions; 5.1.3 Precise determination of lattice constants; 5.1.4 Intensity measurements; 5.2 Area detector diffractometers; 5.2.1 Imaging plates.
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|a 5.2.2 CCD diffractometers5.2.3 Data processing for area detector measurements; 5.2.4 Data collections for B12 and C60F18; 6 Computer programs; 7 Solution of the phase problem; 7.1 Data reduction; 7.2 Fourier methods; 7.2.1 Interpretation of the Patterson function; 7.2.2 Heavy atom methods, principle of difference electron density; 7.2.3 Harker sections, applications to KAMTRA; 7.2.4 Numerical calculation of Fourier syntheses; 7.3 Direct methods; 7.3.1 Normalization; 7.3.2 Fundamental formulae; 7.3.3 Origin definition, choice of starting set.
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|a 7.3.4 Application of direct methods, the examples of SUCROS and C60F187.4 Phase determination for macromolecules; 8 Refinements; 8.1 Theoretical aspects; 8.1.1 Model versus experiment, R-value; 8.1.2 Theory of least-squares refinement; 8.2 Practicing least-squares methods; 8.2.1 Aspects of numerical calculations; 8.2.2 Execution of a complete refinement process; 8.2.3 Corrections to be applied during refinement; 8.3 Analysis and representation of results; 8.3.1 Geometrical data; 8.3.2 Graphical representations; 8.3.3 Archiving data, crystallographic information file (CIF).
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|a This completely revised edition is a guide for practical work in X-ray analysis. Experimental developments e.g. brilliant X-ray sources, area detection, and developments in computer hardware and software have led to increasing applications in X-ray analysis. An introduction to basic crystallography moves quickly to a practical and experimental treatment of structure analysis. Essential reading from the student to the professional level.
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|a Knovel
|b ACADEMIC - Chemistry & Chemical Engineering
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590 |
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|a ProQuest Ebook Central
|b Ebook Central Academic Complete
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590 |
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|a eBooks on EBSCOhost
|b EBSCO eBook Subscription Academic Collection - Worldwide
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|a X-ray crystallography.
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|a Crystallography, X-Ray
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|a Radiocristallographie.
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|a SCIENCE
|x Physics
|x Crystallography.
|2 bisacsh
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|a X-ray crystallography
|2 fast
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|i Print version:
|a Luger, Peter, 1943-
|t Modern X-ray analysis on single crystals.
|b 2nd edition
|z 9783110308235
|w (DLC) 2013045276
|w (OCoLC)862962293
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856 |
4 |
0 |
|u https://ebookcentral.uam.elogim.com/lib/uam-ebooks/detail.action?docID=1575462
|z Texto completo
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