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Inorganic Syntheses.
This volume of Inorganic Syntheses spans the preparations of wide range of important inorganic, organometallic and solid-state compounds. The volume is divided into 6 chapters. The first chapter contains the syntheses of some key early transition metal halide clusters and the very useful mononuclear...
| Clasificación: | Libro Electrónico |
|---|---|
| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Wiley,
2014.
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| Temas: | |
| Acceso en línea: | Texto completo |
MARC
| LEADER | 00000cam a2200000Ma 4500 | ||
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| 003 | OCoLC | ||
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| 100 | 1 | |a Girolami, Gregory S. | |
| 245 | 1 | 0 | |a Inorganic Syntheses. |
| 260 | |b Wiley, |c 2014. | ||
| 300 | |a 1 online resource | ||
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| 588 | 0 | |a Print version record. | |
| 505 | 8 | |a 21. Diruthenium Formamidinato Complexes -- A. Chlorotris(acetato)(N, N'-di-2,6-xylylformamidinato)- diruthenium(II, III) -- B. trans-Chlorobis(acetato)bis(N, N'-di-2,6-xylylformamidinato)- diruthenium(II, III) -- C. cis-Chlorobis(acetato)bis(N, N'-di-p-anisylformamidinato)- diruthenium(II, III) -- D. Chloro(acetato)tris(N, N'-di-p-anisylformamidinato)- diruthenium(II, III) -- E. Chlorotetrakis(N, N'-di-p-anisylformamidinato)- diruthenium(II, III) -- 22. Heptacarbonyl(disulfido)dimanganese(I). -- 23. Di(carbido)tetracosa(carbonyl)decaruthenate(2- ) Salts -- A. Calcium Di(carbido)tetracosa(carbonyl)decaruthenate(2- ) -- B. Bis[bis(triphenylphosphoranylidene)ammonium] Di(carbido)tetracosa(carbonyl)decaruthenate(2- ) -- Chapter Four: General Transition Metal Compounds -- 24. Bis(1,2-bis(dimethylphosphano)ethane)tricarbonyltitanium(0) and Hexacarbonyltitanate(2- ) -- A. Bis(1,2-bis(dimethylphosphano)ethane)- tricarbonyltitanium(0) -- B. Bis[18-crown-6)(acetonitrile)potassium] Hexacarbonyltitanate(2- ) -- 25. Tungsten Benzylidyne Complexes -- A. Trichloro(1,2-dimethoxyethane)benzylidynetungsten(VI) -- B. Chloro Bis[1,2-bis(diphenylphosphino)ethane]- benzylidynetungsten(IV) -- 26. Tungsten Oxytetrachloride and (Acetonitrile)tetrachlorotungsten Imido Complexes -- A. Tungsten Oxytetrachloride -- B. (Acetonitrile)tetrachloro(phenylimido)tungsten(VI) -- C. (Acetonitrile)tetrachloro(2-propylimido)tungsten(VI) -- D. (Acetonitrile)tetrachloro(2-propenylimido)tungsten(VI) -- 27. Tungsten Oxytetrachloride and Several Tungstate Salts -- A. Tungsten Oxytetrachloride -- B. Bis(tetrabutylammonium) Hexapolytungstate -- C. Di(cetylpyridinium) Peroxoditungstate -- D. Bis(tetrabutylammonium) Phenylphosphonatodiperoxotungstate -- 28. Bromotricarbonyldi(pyridine)manganese(I) -- 29. Bis(tetraethylammonium) fac-Tribromotricarbonylrhenate(I) and -Technetate(I). | |
| 520 | |a This volume of Inorganic Syntheses spans the preparations of wide range of important inorganic, organometallic and solid-state compounds. The volume is divided into 6 chapters. The first chapter contains the syntheses of some key early transition metal halide clusters and the very useful mononuclear molybdenum(III) synthon, MoCl3(THF)3. Chapter 2 covers the synthesis of a number of cyclopentadienyl compounds, including a novel route to sodium and potassium cyclopentadienide, MC5H5. Chapter 3 details synthetic procedures for a range of metal-metal bonded compounds, including several with metal-metal multiple bonds. Chapter 4 contains procedures for a range of early and late transition metal compounds, each a useful synthon for further synthetic elaboration. Chapter 5 deals with the synthesis of a number of main group compounds and ligands, while Chapter 6 covers teaching laboratory experiments. | ||
| 590 | |a ProQuest Ebook Central |b Ebook Central Academic Complete | ||
| 650 | 0 | |a Inorganic compounds |x Synthesis. | |
| 650 | 6 | |a Composés inorganiques |x Synthèse. | |
| 650 | 7 | |a Inorganic compounds |x Synthesis |2 fast | |
| 776 | 0 | 8 | |i Print version: |z 9781306533430 |
| 856 | 4 | 0 | |u https://ebookcentral.uam.elogim.com/lib/uam-ebooks/detail.action?docID=1656363 |z Texto completo |
| 880 | 8 | |6 505-00/(S |a A. Bis(tetraethylammonium) fac-Tribromotricarbonylrhenate(I) -- B. Bis(tetraethylammonium) fac-Trichlorotricarbonyltechnetate(I) -- 30. Methyl(oxo)rhenium(V) Complexes with Chelating Ligands -- A. Methyl(oxo)(1,2-ethanedithiolato)rhenium(V) Dimer -- B. Methyl(oxo)bis(2-oxyquinoline)rhenium(V) -- C. Methyl(oxo)(2,2'-thiodiacetato)(triphenylphosphine)- rhenium(V) -- 31. Hexahydridoferrate(II) Salts -- A. Tetrakis[bromobis(tetrahydrofuran)magnesium] Hexahydridoferrate(II) -- B. Tetrakis[2-methyl-2-propoxomagnesium] Hexahydridoferrate(II) -- 32. Tris(allyl)iridium and -Rhodium -- A. Allyllithium -- B. mer-Trichlorotris(tetrahydrothiophene)iridium(III) -- C. mer-Trichlorotris(tetrahydrothiophene)rhodium(III) -- D. Tris(allyl)iridium(III) -- E. Tris(allyl)rhodium(III) -- 33. Trinuclear Palladium(II) Acetate -- Chapter Five: Main Group Compounds and Ligands -- 34. Monocarbaborane Anions with 10 or 12 Vertices -- A. Tetraethylammonium arachno-6-Carba-decaboranate(14) -- B. Tetraethylammonium closo-2-Carba-decaboranate(10) -- C. Tetraethylammonium closo-1-Carba-decaboranate(10) -- D. Tetraethylammonium closo-1-Carba-dodecaboranate(12) -- E. Tetraethylammonium nido-6-Phenyl-6-carbadecaboranate(12) -- F. Tetraethylammonium closo-2-Phenyl-2-carbadecaboranate(10) -- G. Tetraethylammonium closo-1-Phenyl-1-carbadecaboranate(10) -- H. Tetraethylammonium closo-1-Phenyl-1-carbadodecaboranate(12) -- 35. Tetrakis(5-tert-butyl-2-hydroxyphenyl)ethene -- A. 5,5'-Di-tert-butyl-2,2'-dimethoxybenzophenone -- B. Titanium Trichloride 1,2-Dimethoxyethane (1:1.5) -- C. Tetrakis(5-tert-butyl-2-methoxyphenyl)ethene -- D. Tetrakis(5-tert-butyl-2-hydroxyphenyl)ethene -- 36. Electrochemical Synthesis of Tetraethylammonium Tetrathiooxalate -- 37. Mid-Infrared Emitting Lead Selenide Nanocrystal Quantum Dots -- A. Lead Selenide NQDs Emitting at 2.5 μm (0.50 eV). | |
| 880 | 8 | |6 505-00/(S |a E. (μ2-η2,η2-Molybdato)bis[tris(N, N'-di-p-anisylformamidinato)- dimolybdenum(II)] -- F. (μ2-N, N'-Diphenylterephthaloyldiamidato)bis[tris(N, N'-di-panisylformamidinato) dimolybdenum(II)] -- G. Molecular Propeller: (μ3-Trimesate)tris[tris(N, N0-di-panisylformamidinato) dimolybdenum(II)] -- H. Molecular Loop: closo-Bis(μ2-malonato)bis[bis(N, N'-di-panisylformamidinato) dimolybdenum(II)] -- I. Molecular Triangle: closo-Tris(μ2-eq, eq-1,4-cyclohexanedicarboxylato) tris[bis(N, N'-di-p-anisylformamidinato)- dimolybdenum(II)] -- J. Molecular Square: closo-Tetrakis(μ2-oxalato)tetrakis[bis(N, N'- di-p-anisylformamidinato)dimolybdenum(II)] -- K. Molecular Cage: closo-Tetrakis(μ3-trimesate)hexakis[bis(N, N'- di-p-anisylformamidinato)dimolybdenum(II)] -- 18. Dimolybdenum and Ditungsten Hexa(alkoxides) -- A. Hexa(tert-butoxy)dimolybdenum(III) -- B. Hexakis(2-trifluoromethyl-2-propoxy)dimolybdenum(III) -- C. Sodium Heptachloropentakis(tetrahydrofuran)ditungstate(III) -- D. Hexa(tert-butoxy)ditungsten(III) -- E. Hexakis(2-trifluoromethyl-2-propoxy)ditungsten(III) -- 19. Linear Trichromium, Tricobalt, Trinickel, and Tricopper Complexes of 2,2'-Dipyridylamide -- A. Dichlorotetrakis(2,2'-dipyridylamido)trichromium(II) -- B. Dichlorotetrakis(2,2'-dipyridylamido)tricobalt(II) -- C. Dichlorotetrakis(2,2'-dipyridylamido)trinickel(II) -- D. Dichlorotetrakis(2,2'-dipyridylamido)tricopper(II) -- E. Bis(acetonitrile)tetrakis(2,2'-dipyridylamido)trichromium(II) Bis(hexafluorophosphate) -- F. Bis(acetonitrile)tetrakis(2,2'-dipyridylamido)tricobalt(II) Bis(hexafluorophosphate) -- G. Bis(acetonitrile)tetrakis(2,2'-dipyridylamido)trinickel(II) Bis(hexafluorophosphate) -- 20. Bis(tetrabutylammonium) Octachloroditechnetate(III) -- A. Tetrabutylammonium Pertechnetate(VII) -- B. Tetrabutylammonium Oxotetrachlorotechnetate(V) -- C. Bis(tetrabutylammonium) Octachloroditechnetate(III). | |
| 880 | 0 | |6 505-00/(S |a Inorganic Syntheses -- Preface -- Dedication -- Notice to Contributors and Checkers -- Toxic Substances and Laboratory Hazards -- Contents -- Chapter One: Transition Metal Halide Compounds -- 1. Octahedral Hexatantalum Halide Clusters -- A. Tetradecachlorohexatantalum Octahydrate -- B. Tetradecabromohexatantalum Octahydrate -- C. Tetrakis(benzyltributylammonium) Octadecachlorohexatantalate -- 2. Octahedral Hexamolybdenum Halide Clusters -- A. Tetradecachlorohexamolybdate Hexahydrate (Chloromolybdic Acid) -- B. Hexamolybdenum Dodecachloride -- 3. Ether Complexes of Molybdenum(III) and Molybdenum(IV) Chlorides -- A. Tetrachlorobis(diethyl ether)molybdenum(IV) -- B. Trichlorotris(tetrahydrofuran)molybdenum(III) -- 4. Octahedral Hexatungsten Halide Clusters -- A. Bis(hydroxonium) Tetradecachlorohexatungstate Heptahydrate (Chlorotungstic Acid) -- B. Hexatungsten Dodecachloride -- 5. Trinuclear Tungsten Halide Clusters -- A. Tritungsten Decachloride -- B. Trisodium Tridecachlorotritungstate -- C. Tris(benzyltributylammonium) Tridecachlorotritungstate -- 6. Crystalline and Amorphous Forms of Tungsten Tetrachloride -- A. Crystalline Tungsten Tetrachloride by Solid-State Reduction -- B. Amorphous Tungsten Tetrachloride by Solution-Phase Reduction -- Chapter Two: Cyclopentadienyl Compounds -- 7. Sodium and Potassium Cyclopentadienide -- A. Sodium Cyclopentadienide -- B. Potassium Cyclopentadienide -- 8. (Pentafluorophenyl)cyclopentadiene and its Sodium Salt -- A. (Pentafluorophenyl)cyclopentadiene -- B. Sodium (Pentafluorophenyl)cyclopentadienide -- 9. Bis(η5-pentamethylcyclopentadienyl) Complexes of Scandium -- A. Bis(η5-pentamethylcyclopentadienyl)chloroscandium -- B. Bis(η5-pentamethylcyclopentadienyl)methylscandium -- C. Bis(η5-pentamethylcyclopentadienyl)phenylscandium -- D. Bis(η5-pentamethylcyclopentadienyl)(o-tolyl)scandium. | |
| 880 | 8 | |6 505-00/(S |a B. Lead Selenide NQDs Emitting at 2.8 μm (0.44 eV). | |
| 880 | 8 | |6 505-00/(S |a 10. Bis(η5-pentamethylcyclopentadienyl) Complexes of Titanium, Zirconium, and Hafnium -- A. Bis(η5-pentamethylcyclopentadienyl)dichlorotitanium(IV) -- B. Bis(η5-pentamethylcyclopentadienyl)dichlorozirconium(IV) -- C. Bis(η5-pentamethylcyclopentadienyl)dichlorohafnium(IV) -- 11. Bis(η5-pentamethylcyclopentadienyl) Complexes of Niobium and Tantalum -- A. Bis(η5-pentamethylcyclopentadienyl)dichlorotantalum(IV) -- B. Bis(η5-pentamethylcyclopentadienyl)dichloroniobium(IV) -- 12. Bis(η5-pentamethylcyclopentadienyl) Complexes of Molybdenum -- A. Bis(pentamethylcyclopentadienyl)dichloromolybdenum(IV) -- B. Bis(pentamethylcyclopentadienyl)dihydridomolybdenum(IV) -- 13. (η5-Cyclopentadienyl)tricarbonylmanganese(I) Complexes -- A. (η5-Cyclopentadienyl)tricarbonylmanganese(I) -- B. (η5-Pentamethylcyclopentadienyl)tricarbonylmanganese(I) -- 14. 1,1'-Diaminoferrocene -- A. 1,1'-Dilithioferrocene N, N, N', N'-Tetramethylethylenediamine -- B. 1,1'-Dibromoferrocene -- C. One-Pot Preparation of 1,1'-Dibromoferrocene from Ferrocene -- D. 1,1'-Diaminoferrocene -- E. 1,1'-Diaminoferrocenium Hexafluorophosphate -- F. 1,1'-Diaminoferrocenium Triflate -- 15. Mono(η5-pentamethylcyclopentadienyl) Complexes of Osmium -- A. Bromoosmic Acid -- B. Bis(η5-pentamethylcyclopentadienyl)tetrabromodiosmium(III) -- C. (η5-Pentamethylcyclopentadienyl)(1,5-cyclooctadiene)- bromoosmium(II) -- Chapter Three: Compounds with Metal-Metal Bonds -- 16. Tetra(acetato)dimolybdenum(II) -- 17. Supramolecular Arrays Based on Dimolybdenum Building Blocks -- A. Tetrakis(N, N'-di-p-anisylformamidinato)dimolybdenum(II) -- B. Tris(N, N'-di-p-anisylformamidinato)di(chloro)- dimolybdenum(II, III) -- C. cis-Bis(N, N'-di-p-anisylformamidinato)tetrakis(acetonitrile)- dimolybdenum(II) Bis(tetrafluoroborate) -- D. (μ2-Succinato)bis[tris(N, N"-di-p-anisylformamidinato)- dimolybdenum(II)]. | |
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