Structure from diffraction methods /

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"Part of the highly successful Inorganic Materials Series, this new title deals with recent advances in the characterisation of crystalline materials. This very timely volume complements the Series which has so far focused on particular classes of materials (synthesis, structures, chemistry and...

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Detalles Bibliográficos
Clasificación:Libro Electrónico
Otros Autores: Bruce, Duncan W. (Editor ), O'Hare, Dermot (Editor ), Walton, Richard I. (Editor )
Formato: Electrónico eBook
Idioma:Inglés
Publicado: Chichester, West Sussex : John Wiley & Sons Ltd, 2014.
Colección:Inorganic materials series.
Temas:
Molecular structure.
X-rays > Diffraction.
Inorganic compounds > Spectra.
Molecular Structure
X-Ray Diffraction
Structure moléculaire.
Rayons X > Diffraction.
Composés inorganiques > Spectre.
molecular structure.
x-ray diffraction.
TECHNOLOGY & ENGINEERING > Material Science.
Inorganic compounds > Spectra
Molecular structure
X-rays > Diffraction
Acceso en línea:Texto completo
Tabla de Contenidos:
  • Cover; Inorganic Materials Series; Title Page; Copyright; Inorganic Materials Series Preface; Preface; List of Contributors; Chapter 1: Powder Diffraction; 1.1 INTRODUCTION; 1.2 THE SIMILARITIES AND DIFFERENCES BETWEEN SINGLE-CRYSTAL XRD AND POWDER XRD; 1.3 QUALITATIVE ASPECTS OF POWDER XRD: 'FINGERPRINTING' OF CRYSTALLINE PHASES; 1.4 QUANTITATIVE ASPECTS OF POWDER XRD: SOME PRELIMINARIES RELEVANT TO CRYSTAL STRUCTURE DETERMINATION; 1.5 STRUCTURE DETERMINATION FROM POWDER XRD DATA; 1.6 SOME EXPERIMENTAL CONSIDERATIONS IN POWDER XRD; 1.7 POWDER NEUTRON DIFFRACTION VERSUS POWDER XRD.
  • 1.8 VALIDATION OF PROCEDURES AND RESULTS IN STRUCTURE DETERMINATION FROM POWDER XRD DATA1.9 MORE DETAILED CONSIDERATION OF THE APPLICATION OF POWDER XRD AS A 'FINGERPRINT' OF CRYSTALLINE PHASES; 1.10 EXAMPLES OF THE APPLICATION OF POWDER XRD IN CHEMICAL CONTEXTS; 1.11 CONCLUDING REMARKS; References; Chapter 2: X-Ray and Neutron Single-Crystal Diffraction; 2.1 Introduction; 2.2 Solid-State Fundamentals; 2.3 Scattering and Diffraction; 2.4 Experimental Methods; 2.5 STRUCTURE SOLUTION; 2.6 Structure Refinement; 2.7 Problem Structures, Special Topics, Validation and Interpretation.
  • Software AcknowledgementsReferences; Chapter 3: PDF Analysis of Nanoparticles; 3.1 INTRODUCTION; 3.2 PAIR DISTRIBUTION FUNCTION; 3.3 DATA COLLECTION STRATEGIES; 3.4 DATA TREATMENT; 3.5 EXAMPLES; 3.6 COMPLEMENTARY TECHNIQUES; References; Chapter 4: Electron Crystallography; 4.1 INTRODUCTION; 4.2 CRYSTAL DESCRIPTION; 4.3 ELECTRON MICROSCOPY; 4.4 ELECTRON DIFFRACTION; 4.5 IMAGING; 4.6 THE EC METHOD OF SOLVING CRYSTAL STRUCTURES; 4.7 OTHER TEM TECHNIQUES; 4.8 CONCLUSION; References; ACKNOWLEDGMENT; Chapter 5: Small-Angle Scattering; 5.1 INTRODUCTION; 5.2 GENERAL PRINCIPLES OF SAS.
  • 5.3 INSTRUMENTAL SET-UP FOR SAXS5.4 INSTRUMENTAL SET-UP FOR SANS; 5.5 ADDITIONAL REQUIREMENTS FOR SAS; 5.6 APPLICATION OF SAS METHODS; 5.7 CONCLUSION; Acknowledgements; References; Index; End User License Agreement.

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