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|a High throughput analysis for food safety /
|c edited by Perry G. Wang, Mark F. Vitha, Jack F. Kay.
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|a Hoboken, New Jersey :
|b John Wiley & Sons, Inc.,
|c [2014]
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|a 1 online resource
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|a text
|b txt
|2 rdacontent
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|a computer
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|a Chemical analysis ;
|v v. 179
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|a Includes index.
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|a Print version record and CIP data provided by publisher.
|
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|a This book focuses on high-throughput analyses for food safety. Because of the contributors domestic and international expertise from industry and government the book appeals to a wider audience. It includes the latest development in rapid screening, with a particular emphasis on the growing use and applicability of a variety of stand-alone mass spectrometry methods as well as using mass spectrometry in hyphenated techniques such as gas chromatograph mass spectrometry (GC-MS) and liquid chromatography mass spectrometry (LC-MS). Readers will be educated to the field of food safety and rapid test.
|
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|a Includes bibliographical references at the end of each chapters and index.
|
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|6 880-01
|a Chemical Analysis: A Series of Monographs on Analytical Chemistry and its Applications; Title Page; Copyright; Preface; Contributors; Chapter 1: Introduction: Basic Principles of Assays to be Covered, Sample Handling, and Sample Processing; 1.1 Introduction; 1.2 Advanced Sample Preparation Techniques; 1.3 Future Perspectives; Acknowledgment; References; Chapter 2: Survey of Mass Spectrometry-Based High-Throughput Methods in Food Analysis; 2.1 Introduction; 2.2 Techniques Employing Chromatographic Separation; 2.3 Direct Techniques; 2.4 Concluding Remarks; Acknowledgments; References.
|
505 |
8 |
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|a Chapter 3: Quality Systems, Quality Control Guidelines and Standards, Method Validation, and Ongoing Analytical Quality Control3.1 Introduction; 3.2 Qualitative Screening Methods; 3.3 Elements of the Analytical Workflow; 3.4 Initial Method Validation; 3.5 Ongoing Analytical Quality Control; 3.6 Validation of Qualitative Screening Multiresidue Methods for Veterinary Drug Residues in Foods; 3.7 Conclusions; References; Chapter 4: Deliberate Chemical Contamination and Processing Contamination; 4.1 Introduction; 4.2 Heat-Induced Food Processing Contaminants; 4.3 Packaging Migrants.
|
505 |
8 |
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|a 4.4 Malicious Contamination of FoodReferences; Chapter 5: Multiresidual Determination of 295 Pesticides and Chemical Pollutants in Animal Fat by Gel Permeation Chromatography (GPC) Cleanup Coupled with GC-MS/MS, GC-NCI-MS, and LC-MS/MS; 5.1 Introduction; 5.2 Experiment; 5.3 Results and Discussion; 5.4 Conclusions; References; Chapter 6: Ultrahigh-Performance Liquid Chromatography Coupled with High-Resolution Mass Spectrometry: A Reliable Tool for Analysis of Veterinary Drugs in Food; 6.1 Introduction; 6.2 Veterinary Drug Legislation; 6.3 Analytical Techniques for VD Residue Analysis.
|
505 |
8 |
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|a 6.4 Food Control Applications6.5 Conclusions and Future Trends; Acknowledgments; References; Chapter 7: A Role for High-Resolution Mass Spectrometry in the High-Throughput Analysis and Identification of Veterinary Medicinal Product Residues and of their Metabolites in Foods of Animal Origin; 7.1 Introduction; 7.2 Issues Associated with Veterinary Drug Residues and European Regulations; 7.3 Choosing A Strategy: Targeted or Nontargeted Analysis?
|
505 |
8 |
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|a 7.4 Application Number 1: Identification of Brilliant Green and Its Metabolites in Fish Under High-Resolution Mass Spectral Conditions (Targeted and Nontargeted Approaches)7.5 Application Number 2: Targeted and Nontargeted Screening Approaches for the Identification of Antimicrobial Residues in Meat; 7.6 Conclusions; References; Chapter 8: High-Throughput Analysis of Mycotoxins; 8.1 Introduction; 8.2 Sample Preparation; 8.3 Separation and Detection of Mycotoxins; 8.4 No-Separation Mass Spectrometry-Based Methods; 8.5 Conclusions; Acknowledgments; References; Index; End User License Agreement.
|
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|a ProQuest Ebook Central
|b Ebook Central Academic Complete
|
650 |
|
0 |
|a Food
|x Safety measures.
|
650 |
|
0 |
|a Food
|x Safety measures
|x Government policy.
|
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|
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|a Food adulteration and inspection.
|
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1 |
2 |
|a Food Contamination
|x prevention & control
|
650 |
|
6 |
|a Aliments
|x Sécurité
|x Mesures.
|
650 |
|
6 |
|a Aliments
|x Sécurité
|x Mesures
|x Politique gouvernementale.
|
650 |
|
7 |
|a BUSINESS & ECONOMICS
|x Infrastructure.
|2 bisacsh
|
650 |
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7 |
|a SOCIAL SCIENCE
|x General.
|2 bisacsh
|
650 |
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7 |
|a Food adulteration and inspection
|2 fast
|
650 |
|
7 |
|a Food
|x Safety measures
|2 fast
|
700 |
1 |
|
|a Wang, Perry G.
|
700 |
1 |
|
|a Vitha, Mark F.
|
700 |
1 |
|
|a Kay, Jack F.
|
776 |
0 |
8 |
|i Print version:
|t High throughput analysis for food safety.
|d Hoboken, New Jersey : John Wiley & Sons, Inc., [2014]
|z 9781118396308
|w (DLC) 2013051268
|
830 |
|
0 |
|a Chemical analysis ;
|v v. 179.
|
856 |
4 |
0 |
|u https://ebookcentral.uam.elogim.com/lib/uam-ebooks/detail.action?docID=1765098
|z Texto completo
|
880 |
0 |
0 |
|6 505-01/(S
|g Machine generated contents note:
|g ch. 1
|t Introduction: Basic Principles Of Assays To Be Covered, Sample Handling, And Sample Processing /
|r Perry G. Wang --
|g 1.1.
|t Introduction --
|g 1.1.1.
|t Current Situation and Challenges of Food Safety and Regulations --
|g 1.1.2.
|t Residues and Matrices of Food Analysis and High-Throughput Analysis --
|g 1.1.3.
|t Food Safety Classifications --
|g 1.1.4.
|t "High Throughput" Definition --
|g 1.1.5.
|t Scope of the Book --
|g 1.2.
|t Advanced Sample Preparation Techniques --
|g 1.2.1.
|t Automation of Weighing and Preparing Standard Solutions --
|g 1.2.2.
|t QuEChERS --
|g 1.2.3.
|t Swedish Extraction Technique (SweEt) and Other Fast Sample Preparation Methods --
|g 1.2.4.
|t Turbulent Flow Chromatography --
|g 1.2.5.
|t Pressurized Liquid Extraction --
|g 1.2.6.
|t Automated 96- and 384-Well Formatted Sample Preparation as well as Automated SPE Workstations --
|g 1.2.7.
|t Solid-Phase Microextraction --
|g 1.2.8.
|t Microextraction by Packed Sorbent --
|g 1.2.9.
|t Liquid Extraction Surface Analysis --
|g 1.2.10.
|t Headspace GC --
|g 1.2.11.
|t Summary --
|g 1.3.
|t Future Perspectives --
|t Acknowledgment --
|t References --
|g ch. 2
|t Survey Of Mass Spectrometry-Based High-Throughput Methods In Food Analysis /
|r Perry G. Wang --
|g 2.1.
|t Introduction --
|g 2.2.
|t Techniques Employing Chromatographic Separation --
|g 2.2.1.
|t Gas Chromatography--Mass Spectrometry --
|g 2.2.2.
|t Liquid Chromatography--Mass Spectrometry --
|g 2.3.
|t Direct Techniques --
|g 2.3.1.
|t Matrix-Assisted Laser Desorption/Ionization-Mass Spectrometry --
|g 2.3.2.
|t Headspace (Solid-Phase Microextraction)-Mass Spectrometry E-Nose --
|g 2.3.3.
|t Ambient Desorption/Ionization-Mass Spectrometry --
|g 2.4.
|t Concluding Remarks --
|t Acknowledgments --
|t References --
|g ch. 3
|t Quality Systems, Quality Control Guidelines And Standards, Method Validation, And Ongoing Analytical Quality Control /
|r Stewart Reynolds --
|g 3.1.
|t Introduction --
|g 3.1.1.
|t Quality System Design --
|g 3.1.2.
|t Procedures --
|g 3.1.3.
|t Roles and Responsibilities --
|g 3.1.4.
|t Quality Manual --
|g 3.1.5.
|t Document Control --
|g 3.1.6.
|t Control of Records --
|g 3.1.7.
|t Audits --
|g 3.1.8.
|t Validation of Methodology --
|g 3.1.9.
|t Staff Competency --
|g 3.1.10.
|t Internal Quality Control --
|g 3.1.11.
|t Method Performance Criteria --
|g 3.2.
|t Qualitative Screening Methods --
|g 3.2.1.
|t Selectivity of Mass Spectrometry-Based Methods --
|g 3.2.2.
|t Confirmatory Methods --
|g 3.2.3.
|t Validation of Qualitative Screening Multiresidue Methods for Pesticide Residues in Foods --
|g 3.3.
|t Elements of the Analytical Workflow --
|g 3.3.1.
|t Sample Preparation --
|g 3.3.2.
|t Effects of Sample Processing --
|g 3.3.3.
|t Extraction Efficiency --
|g 3.4.
|t Initial Method Validation --
|g 3.5.
|t Ongoing Analytical Quality Control --
|g 3.5.1.
|t Internal Quality Control --
|g 3.5.2.
|t Proficiency Testing --
|g 3.6.
|t Validation of Qualitative Screening Multiresidue Methods for Veterinary Drug Residues in Foods --
|g 3.6.1.
|t EU Legislation Covering Method Validation for Veterinary Drug Screening --
|g 3.6.2.
|t Determination of Specificity/Selectivity and Detection Capability (CQ) Using the Classical Approach --
|g 3.6.3.
|t Establishment of a Cutoff Level and Calculation of CCβ --
|g 3.6.4.
|t Determination of the Applicability --
|g 3.7.
|t Conclusions --
|t References --
|g ch. 4
|t Deliberate Chemical Contamination And Processing Contamination /
|r Stephen Lock --
|g 4.1.
|t Introduction --
|g 4.2.
|t Heat-Induced Food Processing Contaminants --
|g 4.3.
|t Packaging Migrants --
|g 4.4.
|t Malicious Contamination of Food --
|t References --
|g ch. 5
|t Multiresidual Determination Of 295 Pesticides And Chemical Pollutants In Animal Fat By Gel Permeation Chromatography (GPC) Cleanup Coupled With GC-MS/MS, GC-NCI-MS, AND LC-MS/MS /
|r Guo-Fang Pang --
|g 5.1.
|t Introduction --
|g 5.1.1.
|t Persistent Organic Pollutants --
|g 5.1.2.
|t Polycyclic Aromatic Hydrocarbons --
|g 5.1.3.
|t Polychlorinated Biphenyls --
|g 5.1.4.
|t Phthalate Esters --
|g 5.1.5.
|t Multiclass and Multiresidue Analyses --
|g 5.2.
|t Experiment --
|g 5.2.1.
|t Instruments --
|g 5.2.2.
|t Reagents --
|g 5.2.3.
|t Preparation of Standard Solutions --
|g 5.2.4.
|t Sample Preparation --
|g 5.2.5.
|t Analytical Methods --
|g 5.2.6.
|t Qualitative and Quantitative Determination --
|g 5.3.
|t Results and Discussion --
|g 5.3.1.
|t Selection of GPC Cleanup Conditions --
|g 5.3.2.
|t Selection of Extraction Solvent --
|g 5.3.3.
|t Comparison of Sample Extraction Methods --
|g 5.3.4.
|t Comparison of Sample Cleanup --
|g 5.3.5.
|t Linear Range, LOD, and LOQ --
|g 5.3.6.
|t Recoveries and Precisions --
|g 5.3.7.
|t Actual Sample Analysis --
|g 5.4.
|t Conclusions --
|t References --
|g ch. 6
|t Ultrahigh-Performance Liquid Chromatography Coupled With High-Resolution Mass Spectrometry: A Reliable Tool For Analysis Of Veterinary Drugs In Food /
|r Antonia Garrido Frenich --
|g 6.1.
|t Introduction --
|g 6.2.
|t Veterinary Drug Legislation --
|g 6.3.
|t Analytical Techniques for VD Residue Analysis --
|g 6.3.1.
|t Chromatographic Separation --
|g 6.3.2.
|t High-Resolution Mass Spectrometers --
|g 6.4.
|t Food Control Applications --
|g 6.4.1.
|t Screening Applications --
|g 6.4.2.
|t Confirmation and Quantification Methods --
|g 6.4.3.
|t Comparison Studies --
|g 6.5.
|t Conclusions and Future Trends --
|t Acknowledgments --
|t References --
|g ch. 7
|t Role For High-Resolution Mass Spectrometry In The High-Throughput Analysis And Identification Of Veterinary Medicinal Product Residues And Of Their Metabolites In Foods Of Animal Origin /
|r Jagadeshwar-Reddy Thota --
|g 1.1.
|t Introduction --
|g 7.2.
|t Issues Associated with Veterinary Drug Residues and European Regulations --
|g 7.3.
|t Choosing a Strategy: Targeted or Nontargeted Analysis--
|g 7.3.1.
|t Targeted Analysis Using HRMS --
|g 7.3.2.
|t Nontargeted Analysis Using HRMS: Screening for Unknown Compounds --
|g 7.4.
|t Application Number 1: Identification of Brilliant Green and its Metabolites in Fish under High-Resolution Mass Spectral Conditions (Targeted and Nontargeted Approaches) --
|g 7.5.
|t Application Number 2: Targeted and Nontargeted Screening Approaches for the Identification of Antimicrobial Residues in Meat --
|g 7.6.
|t Conclusions --
|t References --
|g ch. 8
|t High-Throughput Analysis Of Mycotoxins /
|r Tomas Cajka --
|g 8.1.
|t Introduction --
|g 8.1.1.
|t Legislation and Regulatory Limits --
|g 8.1.2.
|t Emerging Mycotoxins --
|g 8.1.3.
|t Analysis of Mycotoxins in the High-Throughput Environment --
|g 8.2.
|t Sample Preparation --
|g 8.2.1.
|t Sampling --
|g 8.2.2.
|t Matrices of Interest --
|g 8.2.3.
|t Extraction of Mycotoxins --
|g 8.2.4.
|t Purification of Sample Extracts --
|g 8.3.
|t Separation and Detection of Mycotoxins --
|g 8.3.1.
|t Liquid Chromatography-Mass Spectrometry-Based Methods --
|g 8.3.2.
|t High-Resolution Mass Spectrometry in Mycotoxins Analysis --
|g 8.4.
|t No-Separation Mass Spectrometry-Based Methods --
|g 8.4.1.
|t Matrix-Assisted Laser Desorption Ionization-Mass Spectrometry --
|g 8.4.2.
|t Ambient Ionization Mass Spectrometry --
|g 8.4.3.
|t Ion Mobility Spectrometry --
|g 8.4.4.
|t Immunochemical Methods --
|g 8.5.
|t Conclusions --
|t Acknowledgments --
|t References.
|
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