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Monitoring Polymerization Reactions : From Fundamentals to Applications.
Offers new strategies to optimize polymer reactions With contributions from leading macromolecular scientists and engineers, this book provides a practical guide to polymerization monitoring. It enables laboratory researchers to optimize polymer reactions by providing them with a better understandin...
| Clasificación: | Libro Electrónico |
|---|---|
| Autor principal: | |
| Formato: | Electrónico eBook |
| Idioma: | Inglés |
| Publicado: |
Wiley,
2013.
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| Temas: | |
| Acceso en línea: | Texto completo |
Tabla de Contenidos:
- TITLE PAGE; COPYRIGHT PAGE; PREFACE; INTRODUCTION; CONTRIBUTORS; SECTION 1: OVERVIEW OF POLYMERIZATION REACTIONS AND KINETICS; 1 FREE RADICAL AND CONDENSATION POLYMERIZATIONS; 1.1 INTRODUCTION; 1.2 FREE RADICAL POLYMERIZATION; 1.3 CONDENSATION POLYMERIZATION; 1.4 CONCLUSIONS; REFERENCES; 2 OVERVIEW OF CONTROLLED/LIVING POLYMERIZATION METHODS OF VINYL MONOMERS; 2.1 SCOPE; 2.2 DEFINITION OF LIVING POLYMERIZATIONS; 2.3 SIGNIFICANCE OF LIVING POLYMERIZATIONS; 2.4 ATTRIBUTES OF A CONTROLLED/LIVING POLYMERIZATIONS; 2.5 THERMODYNAMIC CONSIDERATIONS FOR CONTROLLED/LIVING POLYMERIZATIONS.
- 2.6 TYPES OF LIVING POLYMERIZATIONS2.7 CONTROLLED RADICAL POLYMERIZATIONS; 2.8 ARCHITECTURAL POSSIBILITIES WITH CONTROLLED/LIVING POLYMERIZATION METHODS; 2.9 CONCLUSIONS; ACKNOWLEDGMENTS; REFERENCES; 3 STIMULI-RESPONSIVE POLYMERS VIA CONTROLLED RADICAL POLYMERIZATION; 3.1 INTRODUCTION; 3.2 SYNTHESIS OF STIMULI-RESPONSIVE POLYMERS; 3.3 BLOCK COPOLYMERS IN SOLUTION; 3.4 CROSS-LINKED MICELLES; 3.5 STIMULI-RESPONSIVE COPOLYMERS IN BIOCONJUGATES; 3.6 CONCLUSIONS; ACKNOWLEDGMENTS; REFERENCES.
- 4 REACTIONS IN HETEROGENEOUS MEDIA: EMULSION, MINIEMULSION, MICROEMULSION, SUSPENSION, AND DISPERSION POLYMERIZATION4.1 INTRODUCTION; 4.2 DESCRIPTION OF DIFFERENT POLYMERIZATION TECHNIQUES; 4.3 EMULSION POLYMERIZATION; 4.4 MINIEMULSION POLYMERIZATION; 4.5 MICROEMULSION POLYMERIZATION; 4.6 SUSPENSION POLYMERIZATION; 4.7 DISPERSION POLYMERIZATION; REFERENCES; SECTION 2: POLYMERIZATION CHARACTERIZATION AND MONITORING METHODS; 5 POLYMER CHARACTERISTICS; 5.1 INTRODUCTION; 5.2 POLYMER CONFORMATIONS AND DIMENSIONS; 5.3 MOLECULAR WEIGHT DISTRIBUTIONS (MWDs) AND AVERAGES.
- 5.4 POLYMER HYDRODYNAMIC CHARACTERISTICS5.5 ELECTRICALLY CHARGED POLYMERS AND COLLOIDS; 5.6 THERMODYNAMICS OF POLYMER SOLUTIONS; 5.7 RHEOLOGY; 5.8 CHARACTERISTICS OF POLYMERIZATION REACTIONS; 5.9 SUMMARY; REFERENCES; 6 INFRARED (MIR, NIR), RAMAN, AND OTHER SPECTROSCOPIC METHODS; 6.1 INTRODUCTION; 6.2 FUNDAMENTALS; 6.3 MODEL BUILDING AND CALIBRATION; 6.4 MONITORING AND CONTROL OF POLYMERIZATION REACTIONS; 6.5 CONCLUSIONS; REFERENCES; 7 CALORIMETRY, CONDUCTIVITY, DENSIMETRY, AND RHEOLOGICAL MEASUREMENTS; 7.1 INTRODUCTION; 7.2 REACTION CALORIMETRY; 7.3 CONDUCTIVITY; 7.4 DENSIMETRY.
- 7.5 RHEOLOGICAL SENSORS7.6 CONCLUSIONS; REFERENCES; 8 LIGHT SCATTERING; 8.1 INTRODUCTION; 8.2 DYNAMIC LIGHT SCATTERING; 8.3 STATIC LIGHT SCATTERING; ISOTROPIC SYSTEMS; 8.4 STATIC LIGHT SCATTERING: ANISOTROPIC SYSTEMS; 8.5 NOMENCLATURE; REFERENCES; 9 GPC/SEC AS A KEY TOOL FOR ASSESSMENT OF POLYMER QUALITY AND DETERMINATION OF MACROMOLECULAR PROPERTIES; 9.1 INTRODUCTION; 9.2 BASIC CONCEPTS OF SEC; 9.3 SEC ASPECTS OF SEPARATION; 9.4 SEC ASPECTS OF DETECTION; 9.5 COMPREHENSIVE 2D CHROMATOGRAPHY; REFERENCES.