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Industrial Crystallization Process Monitoring and Control.

This ready reference and handbook draws on the experience and expertise of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble...

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Detalles Bibliográficos
Clasificación:Libro Electrónico
Autor principal: Chianese, Angelo
Otros Autores: Kramer, Herman J.
Formato: Electrónico eBook
Idioma:Inglés
Publicado: Hoboken : John Wiley & Sons, 2012.
Temas:
Acceso en línea:Texto completo

MARC

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100 1 |a Chianese, Angelo. 
245 1 0 |a Industrial Crystallization Process Monitoring and Control. 
260 |a Hoboken :  |b John Wiley & Sons,  |c 2012. 
300 |a 1 online resource (253 pages) 
336 |a text  |b txt  |2 rdacontent 
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505 0 |a Industrial Crystallization ProcessMonitoring and Control; Contents; Preface; Scope of the Book; List of Contributors; 1 Characterization of Crystal Size Distribution; 1.1 Introduction; 1.2 Particle Size Distribution; 1.3 Particle Size Distribution Moments; 1.4 Particle Size Distribution Characterization on the Basis of Mass Distribution; References; 2 Forward Light Scattering; 2.1 Introduction; 2.2 Principles of Laser Diffraction; 2.3 Scatter Theory; 2.3.1 Generalized Lorenz-Mie Theory; 2.3.2 Anomalous Diffraction; 2.3.3 Fraunhofer Diffraction; 2.4 Deconvolution. 
505 8 |a 2.4.1 Direct Inversion Using the Nonnegativity Constraint2.4.2 Philips Twomey Inversion Method; 2.4.3 Iterative Methods; 2.5 The Effects of Shape; 2.6 Multiple Scattering; 2.7 Application of Laser Diffraction for Monitoring and Control of Industrial Crystallization Processes; 2.8 Conclusions; References; Further Reading; 3 Focused Beam Reflectance Measurement; 3.1 Measurement Principle; 3.2 Application Examples; 3.2.1 Solubility and Metastable Zone Width (MSZW); 3.2.2 Seed Effectiveness; 3.2.3 Polymorph Transformations; 3.2.4 Effect of Different Impurity Levels; 3.2.5 Nucleation Kinetics. 
505 8 |a 3.2.6 Improved Downstream Processing3.2.7 Process Control; 3.3 Advantages and Limitations; References; 4 Turbidimetry for the Estimation of Crystal Average Size; 4.1 Introduction; 4.2 Determination of Average Particle Size from Specific Turbidity; 4.3 Procedure to Evaluate Average Crystal Size by Turbidimetry for a High Solid Slurry Concentration; 4.4 Conclusion; References; Further Reading; 5 Imaging; 5.1 Introduction; 5.2 Literature Overview; 5.3 The Sensor Design; 5.3.1 Optics and Illumination; 5.3.2 The Camera System and the Resolution; 5.3.3 Image Analysis; 5.3.4 Statistics. 
505 8 |a 5.4 Application of In Situ Imaging for Monitoring Crystallization Processes5.4.1 Example 1; 5.4.2 Example 2; 5.5 Conclusions; References; Further Reading; 6 Turbidimetry and Nephelometry; 6.1 Introduction; 6.2 Measurement of Nucleation and Solubility Points; 6.3 The Developed Turbidimetric and Nephelometric Instruments; 6.4 The Examined Systems; 6.5 Obtained Results; References; 7 Speed of Sound; 7.1 Introduction; 7.2 In-Process Ultrasound Measurement; 7.3 Determining Solubility and Metastable Zone Width; 7.4 Measuring Crystal Growth Rates; 7.5 Detecting Phase Transitions with Ultrasound. 
504 |a References8 In-Line Process Refractometer for Concentration Measurement in Sugar Crystallizers; 8.1 Introduction; 8.2 Measurement Principle; 8.3 In-Line Instrument Features and Benefits; 8.3.1 Accuracy; 8.3.2 Concentration Determination; 8.3.3 Process Temperature Compensation Factor; 8.3.4 Process Sensor; 8.4 Features and Benefits; 8.5 Example of Application in the Crystallization; 8.5.1 Seeding Point and Supersaturation Control in Sugar Vacuum Pan; 8.6 Conclusion; References; 9 ATR-FTIR Spectroscopy; 9.1 Introduction; 9.2 Calibration; 9.3 Speciation Monitoring; 9.4 Co-Crystal Formation. 
500 |a 9.5 Solubility Measurement. 
520 |a This ready reference and handbook draws on the experience and expertise of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. The first part of the book presents the instrumentation and techniques used to measure the crystal size distribution, the nucleation point and solubility point, and the chemical composition of the solid. 
588 0 |a Print version record. 
546 |a English. 
590 |a ProQuest Ebook Central  |b Ebook Central Academic Complete 
650 0 |a Crystallization  |x Industrial applications. 
650 0 |a Process control. 
650 6 |a Cristallisation  |x Applications industrielles. 
650 6 |a Fabrication  |x Contrôle. 
650 7 |a Crystallization  |x Industrial applications  |2 fast 
650 7 |a Process control  |2 fast 
700 1 |a Kramer, Herman J. 
758 |i has work:  |a Industrial crystallization process monitoring and control (Text)  |1 https://id.oclc.org/worldcat/entity/E39PCFGbc3PHdQw4cpYKJmQj83  |4 https://id.oclc.org/worldcat/ontology/hasWork 
776 0 8 |i Print version:  |a Chianese, Angelo.  |t Industrial Crystallization Process Monitoring and Control.  |d Hoboken : John Wiley & Sons, ©2012  |z 9783527331734 
856 4 0 |u https://ebookcentral.uam.elogim.com/lib/uam-ebooks/detail.action?docID=849024  |z Texto completo 
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