Additives in polymers : industrial analysis and applications /

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This industrially relevant resource covers all established and emerging analytical methods for the deformulation of polymeric materials, with emphasis on the non-polymeric components. Each technique is evaluated on its technical and industrial merits.

Detalles Bibliográficos
Clasificación:Libro Electrónico
Autor principal: Bart, Jan C. J.
Formato: Electrónico eBook
Idioma:Inglés
Publicado: Hoboken, NJ : John Wiley, ©2005.
Temas:
Polymers > Additives.
Polymers > Analysis.
Polyme¿¿res > Adjuvants.
Polyme¿¿res > Analyse.
Polymères > Adjuvants.
Polymères > Analyse.
Polymers > Additives
Polymers > Analysis
Acceso en línea:Texto completo
Tabla de Contenidos:
  • ADDITIVES IN POLYMERS Industrial Analysis and Applications; Contents; FOREWORD; PREFACE; ABOUT THE AUTHOR; ACKNOWLEDGEMENTS; CHAPTER 1 Introduction; 1.1 Additives; 1.1.1 Additive functionality; 1.2 Plastics formulations; 1.2.1 Supply forms; 1.2.2 Additive delivery; 1.3 Economic impact of polymer additives; 1.4 Analysis of plastics; 1.4.1 Regulations and standardisation; 1.4.2 Prior art; 1.4.3 Databases; 1.4.4 Scope; 1.4.5 Chapter overview; 1.5 Bibliography; 1.5.1 Plastics additives; 1.5.2 Processing technologies; 1.5.3 Instrumental analysis; 1.5.4 Polymer analysis
  • 1.5.5 Polymer/additive analysis1.6 References; CHAPTER 2 Deformulation Principles; 2.1 Polymer identification; 2.2 Additive analysis of rubbers: 'Best Practice'; 2.3 Polymer extract analysis; 2.4 In situ polymer/additive analysis; 2.5 Class-specific polymer/additive analysis; 2.6 Bibliography; 2.6.1 Polymer identification; 2.6.2 Deformulation of rubbers; 2.6.3 Deformulation of polymers; 2.7 References; CHAPTER 3 Sample Preparation Perspectives; 3.1 Solvents; 3.1.1 Polymer solubility criteria; 3.1.2 Solubility parameters; 3.1.3 Polymer solutions; 3.2 Extraction strategy
  • 3.3 Conventional extraction technologies3.3.1 Liquid-liquid extraction; 3.3.2 Liquid-solid extraction; 3.3.3 Classical solvent extractions of additives from polymers; 3.3.4 Sonication; 3.4 High-pressure solvent extraction methods; 3.4.1 Supercritical fluid technology; 3.4.2 Analytical SFE; 3.4.3 Subcritical water extraction; 3.4.4 Microwave technology; 3.4.5 Microwave-assisted extractions; 3.4.6 Pressurised fluid extraction; 3.5 Sorbent extraction; 3.5.1 Solid-phase extraction; 3.5.2 Solid-phase microextraction; 3.5.3 Stir bar sorptive extraction
  • 3.6 Methodological comparison of extraction methods3.6.1 Experimental comparisons; 3.6.2 Extraction selectivity; 3.6.3 'Nonextractable' additive analysis; 3.7 Polymer/additive dissolution methods; 3.8 Hydrolysis; 3.9 Bibliography; 3.9.1 Sampling and sample preparation; 3.9.2 Solvents/solubility; 3.9.3 Extraction methods; 3.10 References; CHAPTER 4 Separation Techniques; 4.1 Analytical detectors; 4.2 Gas chromatography; 4.2.1 High-temperature gas chromatography; 4.2.2 Headspace gas chromatography; 4.3 Supercritical fluid chromatography; 4.4 Liquid chromatography techniques
  • 4.4.1 Planar chromatographies4.4.2 Column chromatographies; 4.5 Capillary electrophoretic techniques; 4.6 Bibliography; 4.6.1 General texts; 4.6.2 Detectors; 4.6.3 Gas chromatography; 4.6.4 Supercritical fluid chromatography; 4.6.5 Thin-layer chromatography; 4.6.6 Liquid chromatography; 4.6.7 Size-exclusion chromatography; 4.6.8 Ion chromatography; 4.6.9 Capillary electrophoretic techniques; 4.7 References; CHAPTER 5 Polymer/Additive Analysis: The Spectroscopic Alternative; 5.1 Ultraviolet/visible spectrophotometry; 5.2 Infrared spectroscopy; 5.3 Luminescence spectroscopy

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